1,2,4-Trimethyl-9H-carbazole

Base Information

• Chemical Name: 1,2,4-Trimethyl-9H-carbazole
• CAS No.: 97218-74-1
• Molecular Formula: C₁₅H₁₅N
• Molecular Weight: 209.291
• DSSTox Substance ID: DTXSID50548543
• Nikkaji Number: J270.872H
• Wikidata: Q82427282

Synonyms:1,2,4-TRIMETHYL-9H-CARBAZOLE;97218-74-1;DTXSID50548543

Chemical Property of 1,2,4-Trimethyl-9H-carbazole

Chemical Property:

• XLogP3: 4.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 209.120449483
• Heavy Atom Count: 16
• Complexity: 262

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=C2C3=CC=CC=C3NC2=C1C)C

Technology Process of 1,2,4-Trimethyl-9H-carbazole

There total 3 articles about 1,2,4-Trimethyl-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

2-azido-2',4',6'-trimethylbiphenyl (65753-85-7) → 2′,4′,6′-trimethyl-[1,1′-biphenyl]-2-amine (25627-20-7) + 1,2,4-trimethylcarbazole (97218-74-1)

Guidance literature:

With aluminium trichloride; In dichloromethane; Ambient temperature;

DOI:10.1039/c39850000287

Reference yield: 5.0%

2-azido-2',4',6'-trimethylbiphenyl (65753-85-7) → 2′,4′,6′-trimethyl-[1,1′-biphenyl]-2-amine (25627-20-7) + 1,2,4-trimethylcarbazole (97218-74-1) + 2-amino-5-(trifluoromethylsulphonyloxy)-2',4',6'-trimethylbiphenyl (106822-88-2)

Guidance literature:

With trifluorormethanesulfonic acid; In dichloromethane; Ambient temperature;

Reference yield: 5.0%

trifluorormethanesulfonic acid (1493-13-6) + 2-azido-2',4',6'-trimethylbiphenyl (65753-85-7) → 2′,4′,6′-trimethyl-[1,1′-biphenyl]-2-amine (25627-20-7) + 1,2,4-trimethylcarbazole (97218-74-1) + 2-amino-5-(trifluoromethylsulphonyloxy)-2',4',6'-trimethylbiphenyl (106822-88-2)

Guidance literature:

In dichloromethane; Ambient temperature;

upstream raw materials:

trifluorormethanesulfonic acid

2-azido-2',4',6'-trimethylbiphenyl

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