Cyclopentanone, 2-[2-(acetyloxy)-1-oxopropyl]-

Base Information

Chemical Name:Cyclopentanone, 2-[2-(acetyloxy)-1-oxopropyl]-
CAS No.:97315-48-5
Molecular Formula:C10H14O4
Molecular Weight:198.219
Hs Code.:

Synonyms:

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Chemical Property of Cyclopentanone, 2-[2-(acetyloxy)-1-oxopropyl]-

Chemical Property:

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Technology Process of Cyclopentanone, 2-[2-(acetyloxy)-1-oxopropyl]-

There total 1 articles about Cyclopentanone, 2-[2-(acetyloxy)-1-oxopropyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 535-17-1
2-acetoxypropionic acid

: 97315-48-5
(acetoxy-2-propionyl)-2 cyclopentanone

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / 20 °C

2: triethylamine / toluene / Reflux

3: water; acetic acid / tetrahydrofuran / 48 h / 20 °C

With oxalyl dichloride; water; acetic acid; triethylamine; In tetrahydrofuran; toluene;

Reference yield:

: 97315-48-5
(acetoxy-2-propionyl)-2 cyclopentanone

: 1414378-14-5
3-[5-(3,5-dichloro-4-fluoro-phenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-5,6-dihydro-4H-cyclopenta[c]thiophene-1-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrachloromethane; tributylphosphine / 60 °C

1.2: -10 - 0 °C

2.1: manganese(IV) oxide / dichloromethane / 2 h / Reflux

3.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

4.1: thionyl chloride; pyridine / dichloromethane / 3 h / 20 °C

5.1: hydroxylamine hydrochloride; sodium hydroxide / water; tetrahydrofuran / 20 °C

With pyridine; tetrachloromethane; manganese(IV) oxide; thionyl chloride; tributylphosphine; hydroxylamine hydrochloride; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water;

Reference yield:

: 97315-48-5
(acetoxy-2-propionyl)-2 cyclopentanone

: 1414378-26-9
3-[5-(3,5-dichloro-4-fluoro-phenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-5,6-dihydro-4H-cyclopenta[c]thiophene-1-carboxylic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrachloromethane; tributylphosphine / 60 °C

1.2: -10 - 0 °C

2.1: manganese(IV) oxide / dichloromethane / 2 h / Reflux

3.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

4.1: thionyl chloride; pyridine / dichloromethane / 3 h / 20 °C

5.1: hydroxylamine hydrochloride; sodium hydroxide / water; tetrahydrofuran / 20 °C

6.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 0.5 h / 50 °C

6.2: pH 1

With pyridine; tetrachloromethane; manganese(IV) oxide; thionyl chloride; lithium hydroxide monohydrate; tributylphosphine; hydroxylamine hydrochloride; water; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water;