Benzoic acid, 2-iodo-3,4,5-trimethoxy-

Base Information

Chemical Name:Benzoic acid, 2-iodo-3,4,5-trimethoxy-
CAS No.:98799-41-8
Molecular Formula:C10H11IO5
Molecular Weight:338.099
Hs Code.:
NSC Number:118136
DSSTox Substance ID:DTXSID30297789
Nikkaji Number:J2.410.643H
Wikidata:Q82039169

Synonyms:2-iodo-3,4,5-trimethoxybenzoic acid;Benzoic acid, 2-iodo-3,4,5-trimethoxy-;98799-41-8;NSC118136;DTXSID30297789;NSC-118136

Suppliers and Price of Benzoic acid, 2-iodo-3,4,5-trimethoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Benzoic acid, 2-iodo-3,4,5-trimethoxy-

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:337.96512
Heavy Atom Count:16
Complexity:247

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=C(C(=C1)C(=O)O)I)OC)OC

Technology Process of Benzoic acid, 2-iodo-3,4,5-trimethoxy-

There total 5 articles about Benzoic acid, 2-iodo-3,4,5-trimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 118-41-2
Eudesmic acid

: 98799-41-8
2-iodo-3,4,5-trimethoxybenzoic acid

Guidance literature:: With iodine; silver trifluoroacetate; In chloroform; for 3h;
DOI:10.1021/jo0347361

Reference yield:

: 3840-31-1
(3,4,5-trimethoxyphenyl)methanol

: 98799-41-8
2-iodo-3,4,5-trimethoxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: 79 percent / CF₃CO₂Ag; I₂ / CHCl₃ / 1 h / -5 °C

2.1: Jones reagent / acetone; H₂O / 0.08 h / 0 °C

2.2: 91 percent / NaH₂PO₄*2H₂O; H₂O₂; NaClO₂ / acetonitrile; H₂O / 1 h / 20 °C

With jones reagent; iodine; silver trifluoroacetate; In chloroform; water; acetone;
DOI:10.1016/j.tet.2006.10.059

Reference yield:

: 665004-29-5
6,6'-bis(2-iodo-3,4,5-trimethoxybenzyl 1,3-benzodioxole-5-carboxylate)

: 98799-41-8
2-iodo-3,4,5-trimethoxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: 46 mg / DIBAL / toluene / 1 h / -78 °C

2.1: Jones reagent / acetone; H₂O / 0.08 h / 0 °C

2.2: 91 percent / NaH₂PO₄*2H₂O; H₂O₂; NaClO₂ / acetonitrile; H₂O / 1 h / 20 °C

With jones reagent; diisobutylaluminium hydride; In water; acetone; toluene;
DOI:10.1016/j.tet.2006.10.059