2,3-dimethoxy-5-methoxymethoxymethylphenyl 2-iodo-3,4,5-trimethoxybenzoate

Base Information

Chemical Name:2,3-dimethoxy-5-methoxymethoxymethylphenyl 2-iodo-3,4,5-trimethoxybenzoate
CAS No.:1073796-67-4
Molecular Formula:C₂₁H₂₅IO₉
Molecular Weight:548.329
Hs Code.:

Synonyms:2,3-dimethoxy-5-methoxymethoxymethylphenyl 2-iodo-3,4,5-trimethoxybenzoate

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Chemical Property of 2,3-dimethoxy-5-methoxymethoxymethylphenyl 2-iodo-3,4,5-trimethoxybenzoate

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Technology Process of 2,3-dimethoxy-5-methoxymethoxymethylphenyl 2-iodo-3,4,5-trimethoxybenzoate

There total 1 articles about 2,3-dimethoxy-5-methoxymethoxymethylphenyl 2-iodo-3,4,5-trimethoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 925203-40-3
2,3-dimethoxy-5-methoxymethoxymethylphenol

: 98799-41-8
2-iodo-3,4,5-trimethoxybenzoic acid

: 1073796-67-4
2,3-dimethoxy-5-methoxymethoxymethylphenyl 2-iodo-3,4,5-trimethoxybenzoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.3987/COM-08-S(N)8

Reference yield:

: 1073796-67-4
2,3-dimethoxy-5-methoxymethoxymethylphenyl 2-iodo-3,4,5-trimethoxybenzoate

: methyl 2,3-di-O-benzyl-6-O-[3,4,5-trimethoxy-2-(2,3,4-trimethoxy-6-methoxymethoxymethylphenyl)-benzoyl]-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: bis-triphenylphosphine-palladium(II) chloride; sodium acetate / 2,4-dichlorophenoxyacetic acid dimethylamine / 5 h / 120 °C

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 °C

3: potassium carbonate / acetone / 5 h / Reflux

With bis-triphenylphosphine-palladium(II) chloride; sodium acetate; sodium hydride; potassium carbonate; In 2,4-dichlorophenoxyacetic acid dimethylamine; N,N-dimethyl-formamide; acetone; mineral oil;
DOI:10.3987/COM-08-S(N)8