Ruthenium, bis(benzaldehyde)dichloro(triphenylarsine)-

Base Information

Chemical Name:Ruthenium, bis(benzaldehyde)dichloro(triphenylarsine)-
CAS No.:99449-46-4
Molecular Formula:C₃₂H₂₇AsCl₂O₂Ru
Molecular Weight:690.463
Hs Code.:

Synonyms:

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Chemical Property of Ruthenium, bis(benzaldehyde)dichloro(triphenylarsine)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Ruthenium, bis(benzaldehyde)dichloro(triphenylarsine)-

There total 2 articles about Ruthenium, bis(benzaldehyde)dichloro(triphenylarsine)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14898-67-0
ruthenium trichloride hydrate

: 603-32-7
triphenyl-arsane

: 100-52-7
benzaldehyde

: 99449-46-4
[RuCl₂Asph₃(benzaldehyde)2]

Guidance literature:: In butan-1-ol; to soln. of RuCl3*xH2O in n-butanol benzaldehyde is added, soln. of AsPh3 in n-butanol is added to hot soln. and refluxed for 30 min; react. mixt. is cooled overnight, centrifugation, washed with methanol and Et2O and dried under vac.; elem. anal.;
DOI:10.1016/S0277-5387(00)86973-9

Reference yield:

: 14898-67-0
ruthenium(III) chloride trihydrate

: 603-32-7
triphenyl-arsane

: 100-52-7
benzaldehyde

: 99449-46-4
[RuCl₂Asph₃(benzaldehyde)2]

Guidance literature:: In ethanol; RuCl3 in ethanol mixed with aldehyde and triphenylarsine in ethanol under stirring, refluxed for 2 h; ppt. separated out, filtered off, washed with ethanol, dried in vac.; elem. anal.;
DOI:10.1016/S1386-1425(03)00191-4

Reference yield:

: 99449-46-4
[RuCl₂Asph₃(benzaldehyde)2]

: 99449-49-7
(Ru(As(C₆H₅)3)(C₅NH₅)3Cl₂)

Guidance literature:: With pyridine; In pyridine; heating of (Ru(AsPh3)(benz)2Cl2) and py on water-bath for 1 h; soln. is cooled, Et2O is added, mixt. is kept overnight, centrifuged, washed with ether and dried under vac.; elem. anal.;
DOI:10.1016/S0277-5387(00)86973-9