LithiuMsulfate

Base Information

• Chemical Name: LithiuMsulfate
• CAS No.: 1210273-37-2
• Molecular Formula: C8H17ClN2O2
• Molecular Weight: 208.688
• Hs Code.: 2933990090
• Mol file: 1210273-37-2.mol

Synonyms:tert-butyl 3-aminoazetidine-1-carboxylate,hydrochloride;

Chemical Property of LithiuMsulfate

Chemical Property:

• PSA: 55.56000
• LogP: 2.00460

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl3-Aminoazetidine-1-carboxylateHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of LithiuMsulfate

There total 1 articles about LithiuMsulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-aminoazetidine-1-carboxylic acid tert-butyl ester (193269-78-2) → tert-butyl 3-aminoazetidine-1-carboxylate hydrochloride (1210273-37-2)

Guidance literature:

With hydrogenchloride; In methanol; ethanol; water; isopropyl alcohol; at 20 ℃;

Reference yield: 75.0%

tert-butyl 3-aminoazetidine-1-carboxylate hydrochloride (1210273-37-2) + 2,4,6-trichlorophenyl-1-benzyl-5-(methylcarbamoyl)-6-oxo-1,6-dihydropyridine-3-carboxylate → tert-butyl 3-(1-benzyl-5-(methylcarbamoyl)-6-oxo-1,6-dihydropyridine-3-carboxamido)azetidine-1-carboxylate

Guidance literature:

With dmap; triethylamine; In tetrahydrofuran; at 45 ℃; for 5h;

Reference yield:

tert-butyl 3-aminoazetidine-1-carboxylate hydrochloride (1210273-37-2) → 1-isopropylazetidin-3-amine dihydrochloride (117546-56-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tris(acetoxy)borohydride / ethanol; dichloromethane / 21.5 h / 20 °C / Large scale

2: hydrogenchloride / methanol; isopropyl alcohol / 3.75 h / 50 °C / Large scale

With hydrogenchloride; sodium tris(acetoxy)borohydride; In methanol; ethanol; dichloromethane; isopropyl alcohol;

DOI:10.1021/op500072b

upstream raw materials:

3-aminoazetidine-1-carboxylic acid tert-butyl ester

Downstream raw materials:

1-isopropylazetidin-3-amine dihydrochloride

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