N'-(2-cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylformimidamide

Base Information

Chemical Name:N'-(2-cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylformimidamide
CAS No.:1269400-04-5
Molecular Formula:C11H12N4O3
Molecular Weight:248.24
Hs Code.:2926909090
European Community (EC) Number:813-618-8
DSSTox Substance ID:DTXSID40693273
Mol file:1269400-04-5.mol

Synonyms:1269400-04-5;N'-(2-cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylformimidamide;N'-(2-Cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylmethanimidamide;Methanimidamide, N'-(2-cyano-5-methoxy-4-nitrophenyl)-N,N-dimethyl-;(E)-N'-(2-cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylformamidine;DTXSID40693273;KRQJJPTWQAWICH-UHFFFAOYSA-N;BCP29088;AKOS015891286;AS-75540;FT-0778071;(E)-N'-(2-cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylformimidamide;N/'-(2-cyano-5-Methoxy-4-nitrophenyl)-N,N-diMethylforMiMidaMide

Suppliers and Price of N'-(2-cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylformimidamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
N'-(2-Cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylformimidamide 95+%
1g
$ 581.00

Alichem
N'-(2-Cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylformimidamide
1g
$ 502.44

Total 15 raw suppliers

Chemical Property of N'-(2-cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylformimidamide

Chemical Property:

Boiling Point:442.4±55.0 °C(Predicted)
PKA:4.19±0.50(Predicted)
PSA：94.44000
Density:1.22±0.1 g/cm3(Predicted)
LogP:2.21968
Storage Temp.:2-8°C
XLogP3:1.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:248.09094026
Heavy Atom Count:18
Complexity:368

Purity/Quality:

97% ^*data from raw suppliers

N'-(2-Cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylformimidamide 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C=NC1=CC(=C(C=C1C#N)[N+](=O)[O-])OC

Technology Process of N'-(2-cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylformimidamide

There total 10 articles about N'-(2-cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylformimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.5%

: 2-amino-4-methoxy-5-nitrobenzonitrile

: 1269400-04-5
N'-(2-cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylmethanimidamide

Guidance literature:: With N,N-dimethyl-formamide dimethyl acetal; In N,N-dimethyl-formamide; at 70 ℃; for 3.5h;

Reference yield:

: 2-amino-4-methoxy-5-nitrobenzonitrile

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 1269400-04-5
N'-(2-cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylmethanimidamide

Guidance literature:: In N,N-dimethyl-formamide; at 70 ℃; for 3.5h;

Reference yield:

: 204254-66-0
2-amino-4-methoxy-5-nitrobenzoic acid

: 1269400-04-5
N'-(2-cyano-5-methoxy-4-nitrophenyl)-N,N-dimethylmethanimidamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / dichloromethane / 2 h / Reflux

1.2: 1 h / 20 °C

2.1: trichlorophosphate / acetonitrile / 4 h / 50 °C

3.1: N,N-dimethyl-formamide / 3.5 h / 70 °C

With thionyl chloride; trichlorophosphate; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;