10-Chloro-10, 11-dihydrodibenz[b,f]thiepin

Base Information

Chemical Name:10-Chloro-10, 11-dihydrodibenz[b,f]thiepin
CAS No.:1725-32-2
Molecular Formula:C14H11ClS
Molecular Weight:246.76
Hs Code.:2934999090
DSSTox Substance ID:DTXSID30513951
Mol file:1725-32-2.mol

Synonyms:1725-32-2;10-Chloro-10, 11-dihydrodibenz[b,f]thiepin;10-Chloro-10, 11-dihydro-dibenz(b,f)thiepin;10-Chloro-10,11-dihydrodibenzo[b,f]thiepine;10-Chloro-10,11-dihydro-dibenz(b,f)thiepin;5-chloro-5,6-dihydrobenzo[b][1]benzothiepine;10-Chloro-10,11-dihydrodibenz[b,f]thiepin;SCHEMBL8169090;DTXSID30513951;NLQGARUWFXXYMD-UHFFFAOYSA-N;AKOS015850538;10-Chlor-10,11-dihydrodibenzo[b,f]thiepin;FT-0766672;C13565;A847253

Suppliers and Price of 10-Chloro-10, 11-dihydrodibenz[b,f]thiepin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
10-Chloro-10 11-dihydrodibenz[b,f]thiepin95+%
1g
$ 1647.00

Matrix Scientific
10-Chloro-10 11-dihydrodibenz[b,f]thiepin95+%
250mg
$ 756.00

Crysdot
10-Chloro-10,11-dihydrodibenz[b,f]thiepin 95+%
1g
$ 772.00

Alichem
10-Chloro-10,11-dihydrodibenzo[b,f]thiepine
1g
$ 690.80

AK Scientific
10-Chloro-10,11-dihydrodibenz[b,f]thiepin
250mg
$ 1070.00

Total 17 raw suppliers

Chemical Property of 10-Chloro-10, 11-dihydrodibenz[b,f]thiepin

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Melting Point:84.5 °C
Boiling Point:339.691°C at 760 mmHg
Flash Point:150.543°C
PSA：25.30000
Density:1.3g/cm³
LogP:4.67380
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:246.0269992
Heavy Atom Count:16
Complexity:243

Purity/Quality:

97% ^*data from raw suppliers

10-Chloro-10 11-dihydrodibenz[b,f]thiepin95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1C(C2=CC=CC=C2SC3=CC=CC=C31)Cl

Technology Process of 10-Chloro-10, 11-dihydrodibenz[b,f]thiepin

There total 3 articles about 10-Chloro-10, 11-dihydrodibenz[b,f]thiepin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1898-85-7
dibenzo[b,f]thiepin-10(11H)-one

: 1725-32-2
10-chloro-10,11-dihydro-dibenzo[b,f]thiepine

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol / 0.33 h / 0 °C

2: SOCl₂ / 0.17 h / Ambient temperature

With sodium tetrahydroborate; thionyl chloride; In methanol;
DOI:10.1248/cpb.39.2564