1-Butyl-2,3-dimethylimidazolium hydroxide

Base Information

• Chemical Name: 1-Butyl-2,3-dimethylimidazolium hydroxide
• CAS No.: 483184-44-7
• Molecular Formula: C9H18N2O
• Molecular Weight: 170.25202
• Mol file: 483184-44-7.mol

Synonyms:[BMMIM]OH;1-butyl-2,3-dimethyl imidazolium hydroxide;1-butyl-2,3-dimethylimidazolium hydroxide;

Chemical Property of 1-Butyl-2,3-dimethylimidazolium hydroxide

Chemical Property:

• PSA: 31.87000
• LogP: 1.24430

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Butyl-2,3-dimethylimidazolium hydroxide

There total 4 articles about 1-Butyl-2,3-dimethylimidazolium hydroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.92%

1,2-dimethyl-1H-imidazole (1739-84-0) + sulfuric acid dibutyl ester (625-22-9) → 1-butyl-2,3-dimethylimidazolium hydroxide (483184-44-7)

Guidance literature:

1,2-dimethyl-1H-imidazole; sulfuric acid dibutyl ester; at 45 ℃; for 6h;

With barium hydroxide octahydrate; In water; for 1h;

Reference yield:

3-butyl-1,2-dimethylimidazolium chloride (98892-75-2) → 1-butyl-2,3-dimethylimidazolium hydroxide (483184-44-7)

Guidance literature:

With Amberlite IRA 400, basic form; In water;

DOI:10.1039/c6cp03112a

Reference yield:

1-butyl-2,3-dimethylimidazolium bromide → 1-butyl-2,3-dimethylimidazolium hydroxide (483184-44-7)

Guidance literature:

With silver(l) oxide; In water-d2; at 20 ℃; for 2h; Reagent/catalyst; Solvent; Darkness;

DOI:10.1039/c2ra21637j

upstream raw materials:

3-butyl-1,2-dimethylimidazolium chloride

1,2-dimethyl-1H-imidazole

sulfuric acid dibutyl ester

Refernces

• 1、 Song, Zhibin,Huang, Wei,Zhou, Yan,Tian, Zi-Qi,Li, Zhang-Min,Tao, Duan-Jian. "Thermally regulated molybdate-based ionic liquids toward molecular oxygen activation for one-pot oxidative cascade catalysis". . p. 103 - 109. Retrieved 2020/01/21.
• 2、 Klapiszewski, ?ukasz,Szalaty, Tadeusz J.,Kurc, Beata,Stanisz, Ma?gorzata,Zawadzki, Bartosz,Skrzypczak, Andrzej,Jesionowski, Teofil. "Development of Acidic Imidazolium Ionic Liquids for Activation of Kraft Lignin by Controlled Oxidation: Comprehensive Evaluation and Practical Utility". . p. 361 - 374. Retrieved 2018/06/04.