5-[[4-(diethylamino)phenyl]methylene]-4-oxo-2-thioxo-3-Thiazolidineacetic acid

Base Information

Chemical Name:5-[[4-(diethylamino)phenyl]methylene]-4-oxo-2-thioxo-3-Thiazolidineacetic acid
CAS No.:117648-60-9
Molecular Formula:C16H18N2O3S2
Molecular Weight:350.463
Hs Code.:
Mol file:117648-60-9.mol

Synonyms:3-Carboxymethyl-5-(p-diethylaminobenzylidene)rhodanine;

Suppliers and Price of 5-[[4-(diethylamino)phenyl]methylene]-4-oxo-2-thioxo-3-Thiazolidineacetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-[[4-(diethylamino)phenyl]methylene]-4-oxo-2-thioxo-3-Thiazolidineacetic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-[[4-(diethylamino)phenyl]methylene]-4-oxo-2-thioxo-3-Thiazolidineacetic acid

There total 2 articles about 5-[[4-(diethylamino)phenyl]methylene]-4-oxo-2-thioxo-3-Thiazolidineacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.22%

: 5718-83-2
rhodanine 3-acetic acid

: 120-21-8
4-Diethylaminobenzaldehyde

: 117648-60-9
2-(5-(4-(diethylamino)benzylidene)-4-oxo-2-thioxothiazolidin-3-yl)acetic acid

Guidance literature:: With ammonium acetate; acetic acid; for 4h; Reflux;
DOI:10.1016/j.tetlet.2013.04.012

Reference yield:

: N-carboxymethylsulfanylthiocarbonyl-glycine; monopotassium salt

: 117648-60-9
2-(5-(4-(diethylamino)benzylidene)-4-oxo-2-thioxothiazolidin-3-yl)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water / 0.33 h / 90 °C

2: triethylamine / isopropyl alcohol / 5 h / Molecular sieve; Reflux; Inert atmosphere

With hydrogenchloride; triethylamine; In water; isopropyl alcohol;
DOI:10.1007/s00044-017-1852-7