2-MATHYLPROPYL ALCOHOL-OD

Base Information

• Chemical Name: 2-MATHYLPROPYL ALCOHOL-OD
• CAS No.: 14848-63-6
• Molecular Formula: (CH3)2CH2OD
• Molecular Weight: 75.1149
• Mol file: 14848-63-6.mol

Synonyms:

Chemical Property of 2-MATHYLPROPYL ALCOHOL-OD

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-MATHYLPROPYL ALCOHOL-OD

There total 2 articles about 2-MATHYLPROPYL ALCOHOL-OD which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Isobutane (75-28-5,40921-86-6) + trifluoroacetic acid-d1 (599-00-8) + carbon monoxide (201230-82-2) → Isopropanol-d1 (3979-51-9) + iso-BuOD (14848-63-6) + formic acid-d1 (925-94-0) + trifluoroacetic acid-methyl ester (431-47-0) + isopropyl Trifluoroacetate (400-38-4) + isobutyl trifluoroacetate (17355-83-8)

Guidance literature:

With rhodium(III) chloride; water-d2; oxygen; copper(II) trifluoroacetate; sodium chloride; at 95 ℃; for 2.5h; under 48004.8 Torr; Kinetics; Mechanism; Autoclave; Inert atmosphere;

DOI:10.1134/S0023158410050071

Reference yield:

2-methylpropyl phenyl carbonate (13183-18-1) → iso-BuOD (14848-63-6) + phenol-d1 (1003-66-3)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; water-d2; In dimethylsulfoxide-d6; at 40 ℃; Kinetics; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.joc.6b00441

upstream raw materials:

Isobutane

trifluoroacetic acid-d₁

carbon monoxide

2-methylpropyl phenyl carbonate