ethyl 2-broMo-6-forMyl-4H-thieno[3,2-b]pyrrole-5-carboxylate

Base Information

Chemical Name:ethyl 2-broMo-6-forMyl-4H-thieno[3,2-b]pyrrole-5-carboxylate
CAS No.:1221186-54-4
Molecular Formula:C10H8BrNO3S
Molecular Weight:302.14
Hs Code.:
Mol file:1221186-54-4.mol

Synonyms:ethyl 2-bromo-6-formyl-4H-thieno[3,2-b]pyrrole-5-carboxylate

Suppliers and Price of ethyl 2-broMo-6-forMyl-4H-thieno[3,2-b]pyrrole-5-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynChem
ETHYL 2-BROMO-6-FORMYL-4H-THIENO[3,2-B]PYRROLE-5-CARBOXYLATE 95%
1 g
$ 680.00

Matrix Scientific
Ethyl2-bromo-6-formyl-4H-thieno-[3,2-b]pyrrole-5-carboxylate 97%
1g
$ 1324.00

Matrix Scientific
Ethyl2-bromo-6-formyl-4H-thieno-[3,2-b]pyrrole-5-carboxylate 97%
5g
$ 2674.00

Crysdot
Ethyl2-bromo-6-formyl-4H-thieno[3,2-b]pyrrole-5-carboxylate 95+%
10g
$ 1637.00

Crysdot
Ethyl2-bromo-6-formyl-4H-thieno[3,2-b]pyrrole-5-carboxylate 95+%
5g
$ 1196.00

Crysdot
Ethyl2-bromo-6-formyl-4H-thieno[3,2-b]pyrrole-5-carboxylate 95+%
1g
$ 574.00

Total 9 raw suppliers

Chemical Property of ethyl 2-broMo-6-forMyl-4H-thieno[3,2-b]pyrrole-5-carboxylate

Chemical Property:

PSA：87.40000
LogP:2.98110

Purity/Quality:

98%min ^*data from raw suppliers

ETHYL 2-BROMO-6-FORMYL-4H-THIENO[3,2-B]PYRROLE-5-CARBOXYLATE 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ethyl 2-broMo-6-forMyl-4H-thieno[3,2-b]pyrrole-5-carboxylate

There total 4 articles about ethyl 2-broMo-6-forMyl-4H-thieno[3,2-b]pyrrole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 238749-50-3
ethyl 2-bromothieno<3,2-b>pyrrole-5-carboxylate

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1221186-54-4
ethyl 2-bromo-6-formyl-4H-thieno[3,2-b]pyrrole-5-carboxylate

Guidance literature:: N,N-dimethyl-formamide; With trichlorophosphate; Inert atmosphere; Cooling with ice;

ethyl 2-bromothieno<3,2-b>pyrrole-5-carboxylate; at 60 ℃; Inert atmosphere; Cooling with ice;

Reference yield:

: 238749-50-3
ethyl 2-bromothieno<3,2-b>pyrrole-5-carboxylate

: 93-61-8
N-methyl-N-phenylformamide

: 1221186-54-4
ethyl 2-bromo-6-formyl-4H-thieno[3,2-b]pyrrole-5-carboxylate

Guidance literature:: With trichlorophosphate; In 1,2-dichloro-ethane; at 0 - 85 ℃;

Reference yield:

: 4701-17-1
5-bromo-2-thiophencarboxaldehyde

: 1221186-54-4
ethyl 2-bromo-6-formyl-4H-thieno[3,2-b]pyrrole-5-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium ethanolate / ethanol / 1.5 h / -10 - 0 °C

2: 5,5-dimethyl-1,3-cyclohexadiene / 0.17 h / 160 °C

3: trichlorophosphate / 1,2-dichloro-ethane / 0 - 85 °C

With sodium ethanolate; trichlorophosphate; In 5,5-dimethyl-1,3-cyclohexadiene; ethanol; 1,2-dichloro-ethane;