Iodonium, 1-hexynylphenyl-, salt with 4-methylbenzenesulfonic acid (1:1)

Base Information

Chemical Name:Iodonium, 1-hexynylphenyl-, salt with 4-methylbenzenesulfonic acid (1:1)
CAS No.:94957-42-3
Molecular Formula:C12H14I.C7H7O3S
Molecular Weight:456.344
Hs Code.:

Synonyms:

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Chemical Property of Iodonium, 1-hexynylphenyl-, salt with 4-methylbenzenesulfonic acid (1:1)

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Technology Process of Iodonium, 1-hexynylphenyl-, salt with 4-methylbenzenesulfonic acid (1:1)

There total 4 articles about Iodonium, 1-hexynylphenyl-, salt with 4-methylbenzenesulfonic acid (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 27126-76-7
[hydroxy(tosyloxy)iodo]benzene

: 693-02-7
hex-1-yne

: 94957-42-3
n-hexynyl(phenyl)iodonium tosylate

Guidance literature:: In dichloromethane; -78 deg C to room t., 36 h;
DOI:10.1021/ja00235a034

Reference yield:

: 104-15-4
toluene-4-sulfonic acid

: 94957-42-3
n-hexynyl(phenyl)iodonium tosylate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / acetonitrile / 0.5 h

2: dichloromethane / -78 deg C to room t., 36 h

With toluene-4-sulfonic acid; In dichloromethane; acetonitrile;
DOI:10.1021/ja00235a034

Reference yield:

: 3844-94-8
1-(trimethylsilyl)-1-hexyne

: 536-80-1
iodosylbenzene

: 104-15-4
toluene-4-sulfonic acid

: 94957-42-3
n-hexynyl(phenyl)iodonium tosylate

Guidance literature:: 1-(trimethylsilyl)-1-hexyne; iodosylbenzene; With boron trifluoride diethyl etherate; In chloroform; at 0 - 25 ℃; for 16.0833h; Inert atmosphere;

toluene-4-sulfonic acid; With sodium carbonate; In chloroform; water; at 25 ℃; for 0.416667h; Inert atmosphere;
DOI:10.15227/orgsyn.070.0215