4,4'-Didodecyloxyazoxybenzene

Base Information

• Chemical Name: 4,4'-Didodecyloxyazoxybenzene
• CAS No.: 2312-14-3
• Molecular Formula: C₃₆H₅₈N₂O₃
• Molecular Weight: 566.868
• DSSTox Substance ID: DTXSID70467464
• Mol file: 2312-14-3.mol

Synonyms:4,4'-Didodecyloxyazoxybenzene;2312-14-3;4,4'-DI-N-DODECYLOXYAZOXYBENZENE;(4-dodecoxyphenyl)-(4-dodecoxyphenyl)imino-oxidoazanium;Diazene, 1,2-bis[4-(dodecyloxy)phenyl]-, 1-oxide, (1Z)-;(Z)-1,2-bis(4-(dodecyloxy)phenyl)diazene oxide;4,4'-didodecoxyazoxybenzene;SCHEMBL15939251;DTXSID70467464;Bis(4-dodecyloxyphenyl)diazene oxide;MFCD00059283;AKOS015839885;CS-0435413;D0553;FT-0753337;T70605

Chemical Property of 4,4'-Didodecyloxyazoxybenzene

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 657.843oC at 760 mmHg
• Flash Point: 351.651oC
• PSA: 59.57000
• Density: 0.98g/cm3
• LogP: 12.73490
• XLogP3: 14.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 26
• Exact Mass: 566.44474372
• Heavy Atom Count: 41
• Complexity: 598

Purity/Quality:

98% ^*data from raw suppliers

4,4'-Didodecyloxyazoxybenzene >98.0%(N) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCCOC1=CC=C(C=C1)N=[N+](C2=CC=C(C=C2)OCCCCCCCCCCCC)[O-]

Technology Process of 4,4'-Didodecyloxyazoxybenzene

There total 6 articles about 4,4'-Didodecyloxyazoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

4-dodecyloxy-1-nitrobenzene (65039-18-1) → 4,4'-Di-n-dodecyloxyazoxybenzol (2312-14-3)

Guidance literature:

With bismuth; at 20 ℃; for 3h;

DOI:10.1021/jo0203645

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) → 4,4'-Di-n-dodecyloxyazoxybenzol (2312-14-3)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide

2: 25 percent / bismuth / 3 h / 20 °C

With bismuth; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1021/jo0203645

Reference yield:

1-dodecylbromide (143-15-7) → 4,4'-Di-n-dodecyloxyazoxybenzol (2312-14-3)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide

2: 25 percent / bismuth / 3 h / 20 °C

With bismuth; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1021/jo0203645

upstream raw materials:

4-dodecyloxy-1-nitrobenzene

4-nitro-phenol

1-dodecylbromide

potassium 4-nitrophenolate