1,3,5-Trichloro-2,4,6-triiodobenzene

Base Information

Chemical Name:1,3,5-Trichloro-2,4,6-triiodobenzene
CAS No.:151721-79-8
Molecular Formula:C6Cl3I3
Molecular Weight:559.139
Hs Code.:
DSSTox Substance ID:DTXSID10465308
Nikkaji Number:J2.319.349C
Wikidata:Q82291148

Synonyms:1,3,5-Trichloro-2,4,6-triiodobenzene;151721-79-8;SCHEMBL2234460;YSZC2664;DTXSID10465308;BGA72179;MFCD23135489;AKOS016005444;CS-0324307;T3584;T71820;10.14272/RCCCCPGFWUMWDX-UHFFFAOYSA-N.1;doi:10.14272/RCCCCPGFWUMWDX-UHFFFAOYSA-N.1

Suppliers and Price of 1,3,5-Trichloro-2,4,6-triiodobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 19 raw suppliers

Chemical Property of 1,3,5-Trichloro-2,4,6-triiodobenzene

Chemical Property:

XLogP3:5.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:557.6200
Heavy Atom Count:12
Complexity:122

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1(=C(C(=C(C(=C1I)Cl)I)Cl)I)Cl

Technology Process of 1,3,5-Trichloro-2,4,6-triiodobenzene

There total 2 articles about 1,3,5-Trichloro-2,4,6-triiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 108-70-3,63697-19-8
1,3,5-trichlorobenzene

: 151721-79-8
1,3,5-trichloro-2,4,6-triiodo-benzene

Guidance literature:: With sulfuric acid; iodine; periodic acid; at 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201511877

Reference yield: 84.0%

: 108-70-3,63697-19-8
1,3,5-trichlorobenzene

: 10450-60-9
periodic acid

: 7681-11-0
potassium iodide

: 151721-79-8
1,3,5-trichloro-2,4,6-triiodo-benzene

Guidance literature:: periodic acid; potassium iodide; In sulfuric acid; at 0 ℃; for 1h; Inert atmosphere; Schlenk technique;

1,3,5-trichlorobenzene; In sulfuric acid; at 0 - 20 ℃; for 96h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c4dt02307b

Reference yield: 90.0%

: 151721-79-8
1,3,5-trichloro-2,4,6-triiodo-benzene

: 1066-54-2
trimethylsilylacetylene

: 351014-15-8
1,3,5-trichloro-2,4,6-tris[(trimethylsilyl)ethynyl]benzene

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine; In tetrahydrofuran; at 6 ℃; for 72h; Inert atmosphere; Sealed tube;
DOI:10.1002/anie.201704779