Diphenyl azodicarboxylate

Base Information

Chemical Name:Diphenyl azodicarboxylate
CAS No.:2449-14-1
Molecular Formula:C14H10 N2 O4
Molecular Weight:270.244
Hs Code.:
European Community (EC) Number:219-510-1
NSC Number:111166
DSSTox Substance ID:DTXSID0062426
Mol file:2449-14-1.mol

Synonyms:Diphenyl azodicarboxylate;Diazenedicarboxylic acid, diphenyl ester;2449-14-1;diphenyl diazene-1,2-dicarboxylate;Formic acid, azodi-, diphenyl ester;EINECS 219-510-1;NSC111166;NSC 111166;(E)-Diphenyl diazene-1,2-dicarboxylate;1,2-Diazenedicarboxylic acid, 1,2-diphenyl ester;1071721-68-0;phenyl (NE)-N-phenoxycarbonyliminocarbamate;Formic acid, diphenyl ester;DTXSID0062426;Diphenyl 1,2-diazenedicarboxylate;AKOS022182649;NSC-111166;(E)-1-phenoxy-N-[(phenoxycarbonyl)imino]formamide

Suppliers and Price of Diphenyl azodicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of Diphenyl azodicarboxylate

Chemical Property:

Vapor Pressure:6.93E-06mmHg at 25°C
Boiling Point:377.1°Cat760mmHg
Flash Point:166.5°C
Density:1.23g/cm³
XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:270.06405680
Heavy Atom Count:20
Complexity:324

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:C1=CC=C(C=C1)OC(=O)N=NC(=O)OC2=CC=CC=C2
Isomeric SMILES:C1=CC=C(C=C1)OC(=O)/N=N/C(=O)OC2=CC=CC=C2

Technology Process of Diphenyl azodicarboxylate

There total 5 articles about Diphenyl azodicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 10465-98-2
1,2-hydrazinedicarboxylic acid diphenyl ester

: 2449-14-1
Diphenyl azodicarboxylate

Guidance literature:: With pyridine; bromine; In dichloromethane; Ambient temperature;
DOI:10.1080/00397919708004179

Reference yield: 77.5%

: 10465-98-2
1,2-hydrazinedicarboxylic acid diphenyl ester

: 2449-14-1
azodicarboxylic acid diphenyl ester

Guidance literature:: With pyridine; N-Bromosuccinimide; In toluene; at 20 ℃; for 2h;

Reference yield:

: 1885-14-9
phenyl chloroformate

: 2449-14-1
azodicarboxylic acid diphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N₂H₄*H₂O, aq. Na₂CO₃ / CH₂Cl₂

2: NBS, Py / CH₂Cl₂

With pyridine; N-Bromosuccinimide; sodium carbonate; hydrazine hydrate; In dichloromethane;