3-Nitro-6-phenylpyridin-2-amine

Base Information

• Chemical Name: 3-Nitro-6-phenylpyridin-2-amine
• CAS No.: 102266-15-9
• Molecular Formula: C11H9N3O2
• Molecular Weight: 215.211
• Hs Code.: 2933399090
• DSSTox Substance ID: DTXSID50441747
• Wikidata: Q82258667
• Mol file: 102266-15-9.mol

Synonyms:3-nitro-6-phenylpyridin-2-amine;102266-15-9;2-Amino-3-nitro-6-phenylpyridine;3-Nitro-6-phenyl-2-pyridinamine;2-Pyridinamine, 3-nitro-6-phenyl-;SCHEMBL4059206;DTXSID50441747;XBWMSLRYGXSAKH-UHFFFAOYSA-N;3-nitro-6-phenyl-2-pyridine amine;AMY32756;CS-M3452;MFCD16556297;AKOS022175225;AB70856;GS-5574;FT-0713068;F30099;A896836

Chemical Property of 3-Nitro-6-phenylpyridin-2-amine

Chemical Property:

• Melting Point: 147-149 °C(Solv: ethanol (64-17-5); water (7732-18-5))
• Boiling Point: 412.6±45.0 °C(Predicted)
• PKA: 1.90±0.10(Predicted)
• PSA: 84.73000
• Density: 1.327±0.06 g/cm3(Predicted)
• LogP: 3.34340
• Storage Temp.: 2-8°C
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 1
• Exact Mass: 215.069476538
• Heavy Atom Count: 16
• Complexity: 248

Purity/Quality:

97% ^*data from raw suppliers

3-Nitro-6-phenylpyridin-2-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C2=NC(=C(C=C2)[N+](=O)[O-])N

Technology Process of 3-Nitro-6-phenylpyridin-2-amine

There total 7 articles about 3-Nitro-6-phenylpyridin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1,1-diamino-2-nitroethene (71090-35-2) + 3-Dimethylamino-1-phenyl-2-propen-1-on (31919-75-2) → 2-amino-3-nitro-6-phenylpyridine (102266-15-9)

Guidance literature:

With acetic acid; In ethanol; for 4h; Heating;

Reference yield: 75.0%

2-amino-6-chloro-3-nitropyridine (27048-04-0) + phenylboronic acid (98-80-6) → 2-amino-3-nitro-6-phenylpyridine (102266-15-9)

Guidance literature:

2-amino-6-chloro-3-nitropyridine; phenylboronic acid; With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate monohydrate; In water; toluene; for 0.333333h; Inert atmosphere;

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In water; toluene; Inert atmosphere; Reflux;

Reference yield: 65.0%

3-Dimethylamino-1-phenyl-2-propen-1-on (31919-75-2) + 1,1-di(methylsulfanyl)-2-nitroethylene (13623-94-4) → 2-amino-3-nitro-6-phenylpyridine (102266-15-9)

Guidance literature:

With ammonium acetate; In ethanol; for 6h; Heating;

upstream raw materials:

3-Dimethylamino-1-phenyl-2-propen-1-on

1,1-di(methylsulfanyl)-2-nitroethylene

1,1-diamino-2-nitroethene

nitroacetamidine

Downstream raw materials:

2,3-Diamino-6-phenylpyridin

C₃₀H₃₀N₆O₅

tert-butyl (1-(4-((3-nitro-6-phenylpyridin-2-yl)amino)phenyl)cyclobutyl)carbamate

3-(3-(4-(1-aminocyclobutyl)phenyl)-5-phenyl-3H-imidazo[4,5-b]pyridin-2-yl)pyridin-2-amine

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