4-(ethylsulfonyl)-N1-methylbenzene-1,2-diamine

Base Information

Chemical Name:4-(ethylsulfonyl)-N1-methylbenzene-1,2-diamine
CAS No.:68502-19-2
Molecular Formula:C9H14N2O2S
Molecular Weight:214.288
Hs Code.:2921590090
Mol file:68502-19-2.mol

Synonyms:4-(ethylsulfonyl)-N1-methylbenzene-1,2-diamine;5-(Ethylsulfonyl)-2-(MethylaMino)phenylaMine

Suppliers and Price of 4-(ethylsulfonyl)-N1-methylbenzene-1,2-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
4-(Ethylsulfonyl)-N1-methylbenzene-1,2-diamine
1g
$ 444.72

American Custom Chemicals Corporation
4-(ETHYLSULFONYL)-N1-METHYLBENZENE-1,2-DIAMINE 95.00%
5MG
$ 501.12

Crysdot
4-(Ethylsulfonyl)-N1-methylbenzene-1,2-diamine 95+%
1g
$ 535.00

Total 11 raw suppliers

Chemical Property of 4-(ethylsulfonyl)-N1-methylbenzene-1,2-diamine

Chemical Property:

PSA：80.57000
LogP:2.83910
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-(Ethylsulfonyl)-N1-methylbenzene-1,2-diamine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-(ethylsulfonyl)-N1-methylbenzene-1,2-diamine

There total 4 articles about 4-(ethylsulfonyl)-N1-methylbenzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21355-86-2
(4-Ethanesulfonyl-2-nitro-phenyl)-methyl-amine

: 68502-19-2
N¹-methyl-4-ethylsulfonyl-benzene-1,2-diamine

Guidance literature:: (reduction);

Reference yield:

: 7205-80-3
1-(ethylsulfonyl)-4-chlorobenzene

: 68502-19-2
N¹-methyl-4-ethylsulfonyl-benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium nitrate; sulfuric acid / 2 h / 90 °C

2: ethanol / 3 h / 80 °C

3: hydrogen; palladium 10% on activated carbon / ethanol / 3 h / 20 °C / 2068.65 Torr

With sulfuric acid; palladium 10% on activated carbon; hydrogen; potassium nitrate; In ethanol;
DOI:10.1016/j.bioorg.2020.103929

Reference yield:

: 98-60-2
4-chlorobenzenesulfonyl chloride

: 68502-19-2
N¹-methyl-4-ethylsulfonyl-benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 4 steps

1: 90 °C

2: potassium nitrate; sulfuric acid / 2 h / 90 °C

3: ethanol / 3 h / 80 °C

4: hydrogen; palladium 10% on activated carbon / ethanol / 3 h / 20 °C / 2068.65 Torr

With sulfuric acid; palladium 10% on activated carbon; hydrogen; potassium nitrate; In ethanol;
DOI:10.1016/j.bioorg.2020.103929