5-BROMO-2-(2-METHYL-1,3-DIOXOLAN-2-YL)PYRIDINE

Base Information

Chemical Name:5-BROMO-2-(2-METHYL-1,3-DIOXOLAN-2-YL)PYRIDINE
CAS No.:214701-33-4
Molecular Formula:C9H10BrNO2
Molecular Weight:244.088
Hs Code.:2932999099
Mol file:214701-33-4.mol

Synonyms:5-Bromo-2-(2-methyl-1,3-dioxolan-2-yl)pyridine; Pyridine, 5-bromo-2-(2-methyl-1,3-dioxolan-2-yl)-

Suppliers and Price of 5-BROMO-2-(2-METHYL-1,3-DIOXOLAN-2-YL)PYRIDINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

J&W Pharmlab
5-Bromo-2-(2-methyl-[1,3]dioxolan-2-yl)-pyridine 97%
1g
$ 998.00

Crysdot
5-Bromo-2-(2-methyl-1,3-dioxolan-2-yl)pyridine 95+%
250mg
$ 312.00

Crysdot
5-Bromo-2-(2-methyl-1,3-dioxolan-2-yl)pyridine 95+%
1g
$ 780.00

Chemenu
5-bromo-2-(2-methyl-1,3-dioxolan-2-yl)pyridine 95%
1g
$ 729.00

American Custom Chemicals Corporation
5-BROMO-2-(2-METHYL-1,3-DIOXOLAN-2-YL)PYRIDINE 95.00%
5G
$ 2194.50

Alichem
5-Bromo-2-(2-methyl-1,3-dioxolan-2-yl)pyridine
1g
$ 653.12

Total 13 raw suppliers

Chemical Property of 5-BROMO-2-(2-METHYL-1,3-DIOXOLAN-2-YL)PYRIDINE

Chemical Property:

Vapor Pressure:0.003mmHg at 25°C
Boiling Point:294.405°C at 760 mmHg
Flash Point:131.852°C
PSA：31.35000
Density:1.499g/cm³
LogP:2.06360
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

5-Bromo-2-(2-methyl-[1,3]dioxolan-2-yl)-pyridine 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-BROMO-2-(2-METHYL-1,3-DIOXOLAN-2-YL)PYRIDINE

There total 2 articles about 5-BROMO-2-(2-METHYL-1,3-DIOXOLAN-2-YL)PYRIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 107-21-1
ethylene glycol

: 214701-49-2
1-(5-bromopyridin-2-yl)ethanone

: 214701-33-4
5-bromo-2-(2-methyl-1,3-dioxolan-2-yl)pyridine

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 3h; Heating;
DOI:10.1016/j.bmc.2005.03.023

Reference yield:

: 111770-80-0
3-bromo-6-(trimethylsilylethynyl)pyridine

: 214701-33-4
5-bromo-2-(2-methyl-1,3-dioxolan-2-yl)pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / Hg(OAc)2; H₂SO₄ / H₂O; acetone / 1 h / Heating

2: 86 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

With sulfuric acid; mercury(II) diacetate; toluene-4-sulfonic acid; In water; acetone; benzene;
DOI:10.1016/j.bmc.2005.03.023

Reference yield:

: 214701-33-4
5-bromo-2-(2-methyl-1,3-dioxolan-2-yl)pyridine

: 98-16-8
3-trifluoromethylaniline

: 1044210-44-7
C₁₆H₁₅F₃N₂O₂

Guidance literature:: With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; In toluene; for 12h; Heating / reflux;