Benzoic acid, 3-[[6-(ethylsulfonyl)-3-pyridinyl]oxy]-5-[(1S)-2-hydroxy-1-methylethoxy]-, compd. with 1,4-diazabicyclo[2.2.2]octane (2:1)

Base Information

Chemical Name:Benzoic acid, 3-[[6-(ethylsulfonyl)-3-pyridinyl]oxy]-5-[(1S)-2-hydroxy-1-methylethoxy]-, compd. with 1,4-diazabicyclo[2.2.2]octane (2:1)
CAS No.:1137917-12-4
Molecular Formula:C17H19NO7S.1/2C6H12N2
Molecular Weight:
Hs Code.:

Synonyms:Benzoic acid, 3-[[6-(ethylsulfonyl)-3-pyridinyl]oxy]-5-[(1S)-2-hydroxy-1-Methylethoxy]-, coMpd. with 1,4-diazabicyclo[2.2.2]octane (2:1)

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Chemical Property of Benzoic acid, 3-[[6-(ethylsulfonyl)-3-pyridinyl]oxy]-5-[(1S)-2-hydroxy-1-methylethoxy]-, compd. with 1,4-diazabicyclo[2.2.2]octane (2:1)

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Technology Process of Benzoic acid, 3-[[6-(ethylsulfonyl)-3-pyridinyl]oxy]-5-[(1S)-2-hydroxy-1-methylethoxy]-, compd. with 1,4-diazabicyclo[2.2.2]octane (2:1)

There total 8 articles about Benzoic acid, 3-[[6-(ethylsulfonyl)-3-pyridinyl]oxy]-5-[(1S)-2-hydroxy-1-methylethoxy]-, compd. with 1,4-diazabicyclo[2.2.2]octane (2:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 280-57-9,88935-43-7
1,4-diaza-bicyclo[2.2.2]octane

: 1137917-10-2
3-(6-ethanesulfonylpyridin-3-yloxy)-5-((S)-2-hydroxy-1-methylethoxy)benzoic acid

: 1137917-12-4
0.5C₆H₁₂N₂*C₁₇H₁₉NO₇S

Guidance literature:: In methanol; Isopropyl acetate; at 50 ℃;

Reference yield: 89.0%

: 280-57-9,88935-43-7
1,4-diaza-bicyclo[2.2.2]octane

: 1137917-10-2
3-(6-ethanesulfonylpyridin-3-yloxy)-5-((S)-2-hydroxy-1-methylethoxy)benzoic acid

: 1137917-12-4
bis[3-(6-ethanesulfonylpyridin-3-yloxy)-5-((S)-2-hydroxy-1-methylethoxy)benzoic acid] 1,4-diazabicyclo[2.2.2]octane salt

Guidance literature:: In Isopropyl acetate; at 22 - 50 ℃; for 15h; Large scale reaction;
DOI:10.1021/op200068c

Reference yield: 71.0%

: 280-57-9,88935-43-7
1,4-diaza-bicyclo[2.2.2]octane

: 752242-66-3
3-((1S)-2-(t-butyldimethylsiloxy)-1-methylethoxy)-5-(6-ethanesulfonylpyridin-3-yloxy)benzoic acid methyl ester

: 1137917-12-4
bis[3-(6-ethanesulfonylpyridin-3-yloxy)-5-((S)-2-hydroxy-1-methylethoxy)benzoic acid] 1,4-diazabicyclo[2.2.2]octane salt

Guidance literature:: 3-((1S)-2-(t-butyldimethylsiloxy)-1-methylethoxy)-5-(6-ethanesulfonylpyridin-3-yloxy)benzoic acid methyl ester; With hydrogenchloride; water; In water;

With sodium hydroxide; In water;

1,4-diaza-bicyclo[2.2.2]octane; In water;
DOI:10.1021/op200068c