(4-(9-phenyl-9H-carbazol-3-yl)phenyl)boronic acid

Base Information

• Chemical Name: (4-(9-phenyl-9H-carbazol-3-yl)phenyl)boronic acid
• CAS No.: 1240963-55-6
• Molecular Formula: C24H18BNO2
• Molecular Weight: 363.223
• Mol file: 1240963-55-6.mol

Synonyms:9-phenyl-9H-carbazol-3-yl-phenyl-4-boronic acid;4-(9-phenyl-9H-carbazol-3-yl)phenylboronicacid;

Chemical Property of (4-(9-phenyl-9H-carbazol-3-yl)phenyl)boronic acid

Chemical Property:

• Boiling Point: 555.9±60.0 °C(Predicted)
• PKA: 8.62±0.17(Predicted)
• PSA: 45.39000
• Density: 1.18±0.1 g/cm3(Predicted)
• LogP: 4.13050
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

98% ^*data from raw suppliers

(4-(9-Phenyl-9h-Carbazol-3-Yl)Phenyl)BoronicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of (4-(9-phenyl-9H-carbazol-3-yl)phenyl)boronic acid

There total 14 articles about (4-(9-phenyl-9H-carbazol-3-yl)phenyl)boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

Trimethyl borate (121-43-7,63156-11-6) + 3-(4-bromophenyl)-9-phenyl-9H-carbazole (1028647-93-9) → 4-(9-phenyl-9H-carbazol-3-yl)phenylboronic acid (1240963-55-6)

Guidance literature:

Trimethyl borate; 3-(4-bromophenyl)-9-phenyl-9H-carbazole; In tetrahydrofuran; at -78 - 20 ℃; for 20h; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; water; for 7h;

Reference yield: 88.0%

3-(4-bromophenyl)-9-phenyl-9H-carbazole (1028647-93-9) → 4-(9-phenyl-9H-carbazol-3-yl)phenylboronic acid (1240963-55-6)

Guidance literature:

3-(4-bromophenyl)-9-phenyl-9H-carbazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;

With Trimethyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 20h;

With hydrogenchloride; In tetrahydrofuran; hexane; water; for 7h;

Reference yield: 88.0%

Trimethyl borate (121-43-7,63156-11-6) + 3-(4-bromophenyl)-9-phenyl-9H-carbazole (1028647-93-9) + water (7732-18-5) → 4-(9-phenyl-9H-carbazol-3-yl)phenylboronic acid (1240963-55-6)

Guidance literature:

3-(4-bromophenyl)-9-phenyl-9H-carbazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 14h; Inert atmosphere;

Trimethyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 20h;

water; With hydrogenchloride; In tetrahydrofuran; hexane; for 7h;

upstream raw materials:

3-(4-bromophenyl)-9-phenyl-9H-carbazole

Trimethyl borate

1,4-bromoiodobenzene

N-phenyl-9H-carbazol-3-boronic acid

Downstream raw materials:

3-[4-(9-phenanthryl)-phenyl]-9-phenyl-9H-carbazole

9-phenyl-3-[4-(triphenylen-2-yl)-phenyl]-9H-carbazole

9-phenyl-9H-3-{4-[3,5-di(phenanthren-9-yl)phenyl]phenyl}carbazole

C₃₆H₂₄N₂

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