Propanamide, 2,2-dimethyl-N-[2-(triethoxysilyl)phenyl]-

Base Information

Chemical Name:Propanamide, 2,2-dimethyl-N-[2-(triethoxysilyl)phenyl]-
CAS No.:776296-16-3
Molecular Formula:C17H29NO4Si
Molecular Weight:339.507
Hs Code.:

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Chemical Property of Propanamide, 2,2-dimethyl-N-[2-(triethoxysilyl)phenyl]-

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Technology Process of Propanamide, 2,2-dimethyl-N-[2-(triethoxysilyl)phenyl]-

There total 3 articles about Propanamide, 2,2-dimethyl-N-[2-(triethoxysilyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 78-10-4
tetraethoxy orthosilicate

: 6625-74-7
N-pivaloylaniline

: 776296-16-3
2-(triethoxysilyl)pivalanilide

Guidance literature:: N-pivaloylaniline; With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane; at 25 ℃; for 20h;

tetraethoxy orthosilicate; In tetrahydrofuran; diethyl ether; hexane; at 20 ℃; for 4h;
DOI:10.1021/jo0492057

Reference yield:

: 3282-30-2
pivaloyl chloride

: 776296-16-3
2-(triethoxysilyl)pivalanilide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 96 percent / Na₂CO₃ / H₂O; CH₂Cl₂ / 1 h / Heating

2.1: n-BuLi / tetrahydrofuran; diethyl ether; hexane / 20 h / 25 °C

2.2: 62 percent / tetrahydrofuran; diethyl ether; hexane / 4 h / 20 °C

With n-butyllithium; sodium carbonate; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water;
DOI:10.1021/jo0492057

Reference yield:

: 62-53-3
aniline

: 776296-16-3
2-(triethoxysilyl)pivalanilide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 96 percent / Na₂CO₃ / H₂O; CH₂Cl₂ / 1 h / Heating

2.1: n-BuLi / tetrahydrofuran; diethyl ether; hexane / 20 h / 25 °C

2.2: 62 percent / tetrahydrofuran; diethyl ether; hexane / 4 h / 20 °C

With n-butyllithium; sodium carbonate; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water;
DOI:10.1021/jo0492057