1-(2,4-Dimethoxyphenyl)-3-phenyl-1,3-propanedione

Base Information

Chemical Name:1-(2,4-Dimethoxyphenyl)-3-phenyl-1,3-propanedione
CAS No.:80370-26-9
Molecular Formula:C17H16O4
Molecular Weight:284.312
Hs Code.:
NSC Number:75523
DSSTox Substance ID:DTXSID501001193
Nikkaji Number:J461.389I
Wikidata:Q82995025

Synonyms:1-(2,4-Dimethoxyphenyl)-3-phenyl-1,3-propanedione;80370-26-9;1-(2,4-dimethoxyphenyl)-3-phenylpropane-1,3-dione;NSC75523;NCIOpen2_004651;DTXSID501001193;NSC 75523;NSC-75523;1,3-Propanedione, 1-(2,4-dimethoxyphenyl)-3-phenyl-

Suppliers and Price of 1-(2,4-Dimethoxyphenyl)-3-phenyl-1,3-propanedione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-(2,4-Dimethoxyphenyl)-3-phenyl-1,3-propanedione

Chemical Property:

Vapor Pressure:8.92E-09mmHg at 25°C
Boiling Point:463.7°Cat760mmHg
Flash Point:206.4°C
Density:1.16g/cm³
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:284.10485899
Heavy Atom Count:21
Complexity:360

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C=C1)C(=O)CC(=O)C2=CC=CC=C2)OC

Technology Process of 1-(2,4-Dimethoxyphenyl)-3-phenyl-1,3-propanedione

There total 4 articles about 1-(2,4-Dimethoxyphenyl)-3-phenyl-1,3-propanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 93-89-0,99341-95-4
benzoic acid ethyl ester

: 829-20-9
2',4'-dimethoxyacetophenone

: 80370-26-9
1-(2,4-dimethoxyphenyl)-3-phenyl-1,3-propanedione

Guidance literature:: With sodium hydride; In benzene; for 3h;
DOI:10.1248/cpb.40.1047

Reference yield:

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 829-20-9
2',4'-dimethoxyacetophenone

: 80370-26-9
1-(2,4-dimethoxyphenyl)-3-phenyl-1,3-propanedione

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at 70 ℃; for 8h; Inert atmosphere;
DOI:10.1002/adsc.202001169

Reference yield:

: 91-52-1
2,4 dimethoxybenzoic acid

: 80370-26-9
1-(2,4-dimethoxyphenyl)-3-phenyl-1,3-propanedione

Guidance literature:: Multi-step reaction with 2 steps

1: H₂SO₄

2: diethyl ether; sodium

With diethyl ether; sulfuric acid; sodium;