ethyl 2,4-dimethoxybenzoate

Base Information

• Chemical Name: ethyl 2,4-dimethoxybenzoate
• CAS No.: 81722-07-8
• Molecular Formula: C11H14O4
• Molecular Weight: 210.22600
• Mol file: 81722-07-8.mol

Synonyms:2,4-Dimethoxybenzoesaeuremethylester;ethyl veratrate;2,4-DIMETHOXYBENZOIC ACID ETHYL ESTER;Dimethylaether-β-resorcylsaeure-aethylester;2,4-Dimethoxy-benzoesaeure-aethylester;2,4-dimethoxy-benzoic acid ethyl ester;

Chemical Property of ethyl 2,4-dimethoxybenzoate

Chemical Property:

• PSA: 44.76000
• LogP: 1.88050

Purity/Quality:

99% ^*data from raw suppliers

Ethyl2,4-Dimethoxybenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl 2,4-dimethoxybenzoate

There total 2 articles about ethyl 2,4-dimethoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

ethanol (64-17-5) + 2,4 dimethoxybenzoic acid (91-52-1) → ethyl 2,4-dimethoxybenzoate (81722-07-8)

Guidance literature:

With sulfuric acid; for 3h; Heating;

DOI:10.1248/cpb.40.1047

Reference yield: 55.0%

1,5-dimethoxy-1,4-cyclohexadiene (37567-78-5) + propynoic acid ethyl ester (623-47-2) → ethyl 2,4-dimethoxybenzoate (81722-07-8)

Guidance literature:

With dichloromaleic acid anhydride; at 100 ℃; for 4h;

DOI:10.1055/s-1982-29756

Reference yield: 69.0%

2,5-dimethyl-1,3,4-thiadiazole (27464-82-0) + ethyl 2,4-dimethoxybenzoate (81722-07-8) → 1-(2,4-Dimethoxyphenyl)-2-[5-methyl-1,3,4-thiadiazol-2-yl]ethanon (724454-81-3)

Guidance literature:

2,5-dimethyl-1,3,4-thiadiazole; With sodium hydride; In toluene; at 30 - 60 ℃; for 1h;

ethyl 2,4-dimethoxybenzoate; In toluene; for 4h; Heating;

DOI:10.1515/znb-2004-0403

upstream raw materials:

ethanol

2,4 dimethoxybenzoic acid

1,5-dimethoxy-1,4-cyclohexadiene

propynoic acid ethyl ester

Downstream raw materials:

2,3-bis-(2,4-dimethoxy-phenyl)-3-oxo-propionitrile

1-(2,4-dimethoxyphenyl)-3-phenyl-1,3-propanedione

1-(2,4-Dimethoxyphenyl)-2-[5-methyl-1,3,4-thiadiazol-2-yl]ethanon

2,4,2',4'-tetramethoxy-deoxybenzoin

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