Benzenesulfonamide, N-[2-(acetyloxy)-2-(4-fluorophenyl)ethyl]-N,4-dimethyl-

Base Information

• Chemical Name: Benzenesulfonamide, N-[2-(acetyloxy)-2-(4-fluorophenyl)ethyl]-N,4-dimethyl-
• CAS No.: 450-00-0
• Molecular Formula: C18H20FNO4S
• Molecular Weight: 365.426

Synonyms:p-Toluenesulfonamide, N-(p-fluoro-β-hydroxyphenethyl)-N-methyl-, acetate (8CI);

Chemical Property of Benzenesulfonamide, N-[2-(acetyloxy)-2-(4-fluorophenyl)ethyl]-N,4-dimethyl-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenesulfonamide, N-[2-(acetyloxy)-2-(4-fluorophenyl)ethyl]-N,4-dimethyl-

There total 2 articles about Benzenesulfonamide, N-[2-(acetyloxy)-2-(4-fluorophenyl)ethyl]-N,4-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

para-fluorostyrene (405-99-2) → 1-acetoxy-1-(4-fluoro-phenyl)-2-[methyl-(toluene-4-sulfonyl)-amino]-ethane (450-00-0)

Guidance literature:

With chloroform; Erwaermen des Reaktionsprodukts mit Natriumacetat in Essigsaeure;

DOI:10.1021/ja01209a038

Reference yield:

(2-bromoethyl)-4-fluorobenzene (332-42-3) → 1-acetoxy-1-(4-fluoro-phenyl)-2-[methyl-(toluene-4-sulfonyl)-amino]-ethane (450-00-0)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH / 200 - 220 °C

2: chloroform / Erwaermen des Reaktionsprodukts mit Natriumacetat in Essigsaeure

With potassium hydroxide; chloroform;

DOI:10.1021/ja01209a038

Reference yield:

1-acetoxy-1-(4-fluoro-phenyl)-2-[methyl-(toluene-4-sulfonyl)-amino]-ethane (450-00-0) → N-(4-fluoro-β-hydroxy-phenethyl)-N-methyl-toluene-4-sulfonamide (599-68-8)

Guidance literature:

With sodium hydroxide;

DOI:10.1021/ja01209a038

upstream raw materials:

para-fluorostyrene

(2-bromoethyl)-4-fluorobenzene

Downstream raw materials:

N-(4-fluoro-β-hydroxy-phenethyl)-N-methyl-toluene-4-sulfonamide

1-(4-fluoro-phenyl)-2-methylamino-ethanol

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