5-aMino-2-broMo-4-Methylbenzoic acid Methyl ester

Base Information

• Chemical Name: 5-aMino-2-broMo-4-Methylbenzoic acid Methyl ester
• CAS No.: 474330-54-6
• Molecular Formula: C9H10BrNO2
• Molecular Weight: 244.088
• Mol file: 474330-54-6.mol

Synonyms:5-amino-2-bromo-4-methylbenzoic acid methyl ester;Benzoic acid,5-amino-2-bromo-4-methyl-,methyl ester;QC-9695;

Chemical Property of 5-aMino-2-broMo-4-Methylbenzoic acid Methyl ester

Chemical Property:

• Boiling Point: 328.4±37.0 °C(Predicted)
• PKA: 2.60±0.10(Predicted)
• PSA: 52.32000
• Density: 1.506±0.06 g/cm3(Predicted)
• LogP: 2.70750
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

98% ^*data from raw suppliers

5-Amino-2-bromo-4-methylbenzoic acid methyl ester 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-aMino-2-broMo-4-Methylbenzoic acid Methyl ester

There total 4 articles about 5-aMino-2-broMo-4-Methylbenzoic acid Methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

methanol (67-56-1) + 5-amino-2-bromo-4-methylbenzoic acid (745048-63-9) → 5-amino-2-bromo-4-methylbenzoic acid methyl ester (474330-54-6)

Guidance literature:

With thionyl chloride; for 6h; Heating / reflux;

Reference yield: 95.5%

5-amino-2-bromo-4-methylbenzoic acid (745048-63-9) → 5-amino-2-bromo-4-methylbenzoic acid methyl ester (474330-54-6)

Guidance literature:

With thionyl chloride; In methanol; at 20 ℃; for 2h; Reflux;

Reference yield: 90.0%

3-amino-4-methyl benzoic acid methyl ester (18595-18-1) → 5-amino-2-bromo-4-methylbenzoic acid methyl ester (474330-54-6)

Guidance literature:

With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h;

upstream raw materials:

methanol

5-amino-2-bromo-4-methylbenzoic acid

3-amino-4-methyl benzoic acid methyl ester

3-amino-p-toluic acid

Downstream raw materials:

2-bromo-5-chloro-4-methyl-benzoic acid methyl ester

C₉H₈BrFO₂

methyl 4-(acetoxymethyl)-2-bromo-5-chlorobenzoate

methyl 2-bromo-4-(bromomethyl)-5-chlorobenzoate

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