5-BENZYLOXY-2-NITRO-PHENYLACETALDEHYDE

Base Information

Chemical Name:5-BENZYLOXY-2-NITRO-PHENYLACETALDEHYDE
CAS No.:705961-42-8
Molecular Formula:C15H13NO4
Molecular Weight:271.26802
Hs Code.:
Mol file:705961-42-8.mol

Synonyms:5-BENZYLOXY-2-NITRO-PHENYLACETALDEHYDE;3-BENZYLOXY-6-NITRO-PHENYLACETALDEHYDE;Benzeneacetaldehyde, 2-nitro-5-(phenylmethoxy)-

Suppliers and Price of 5-BENZYLOXY-2-NITRO-PHENYLACETALDEHYDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-BENZYLOXY-6-NITRO-PHENYLACETALDEHYDE 95.00%
5MG
$ 498.44

Total 2 raw suppliers

Chemical Property of 5-BENZYLOXY-2-NITRO-PHENYLACETALDEHYDE

Chemical Property:

PSA：72.12000
LogP:3.43840

Purity/Quality:

98% ^*data from raw suppliers

3-BENZYLOXY-6-NITRO-PHENYLACETALDEHYDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-BENZYLOXY-2-NITRO-PHENYLACETALDEHYDE

There total 3 articles about 5-BENZYLOXY-2-NITRO-PHENYLACETALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 22424-58-4
5-benzyloxy-2-nitrotoluene

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 705961-42-8
(5-benzyloxy-2-nitrophenyl)-acetaldehyde

Guidance literature:: 5-benzyloxy-2-nitrotoluene; N,N-dimethyl-formamide dimethyl acetal; In N,N-dimethyl-formamide; for 24h; Heating;

With hydrogenchloride; In diethyl ether; for 2h; Further stages.; Heating;
DOI:10.1039/b400110a

Reference yield:

: 2581-34-2,910311-23-8
3-methyl-4-nitrophenol

: 705961-42-8
(5-benzyloxy-2-nitrophenyl)-acetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: 91 percent / K₂CO₃ / dimethylformamide / 2 h / 90 °C

2.1: dimethylformamide / 24 h / Heating

2.2: 82 percent / aq. HCl / diethyl ether / 2 h / Heating

With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1039/b400110a

Reference yield:

: 100-39-0
benzyl bromide

: 705961-42-8
(5-benzyloxy-2-nitrophenyl)-acetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: 91 percent / K₂CO₃ / dimethylformamide / 2 h / 90 °C

2.1: dimethylformamide / 24 h / Heating

2.2: 82 percent / aq. HCl / diethyl ether / 2 h / Heating

With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1039/b400110a