Methyl 2-azetidinecarboxylate hydrochloride

Base Information

• Chemical Name: Methyl 2-azetidinecarboxylate hydrochloride
• CAS No.: 162698-26-2
• Molecular Formula: C5H9NO2.ClH
• Molecular Weight: 151.593
• Hs Code.: 2933998090
• Mol file: 162698-26-2.mol

Synonyms:2-Azetidinecarboxylic acid, Methyl ester, hydrochloride

Chemical Property of Methyl 2-azetidinecarboxylate hydrochloride

Chemical Property:

• PSA: 38.33000
• LogP: 0.65210
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

MethylAzetidine-2-carboxylateHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 2-azetidinecarboxylate hydrochloride

There total 2 articles about Methyl 2-azetidinecarboxylate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

methanol (67-56-1) + Azetidine-2-carboxylic acid (2517-04-6,20063-89-2) → azetidine-2-carboxylic acid methyl ester hydrochloride (162698-26-2,51020-00-9)

Guidance literature:

methanol; With thionyl chloride; at 0 ℃;

Azetidine-2-carboxylic acid; at 20 ℃;

Reference yield:

(2S)-Methyl-1-azetidine-2-carboxylic acid (255882-95-2) → azetidine-2-carboxylic acid methyl ester hydrochloride (162698-26-2,51020-00-9)

Guidance literature:

With thionyl chloride; In methanol;

Reference yield: 71.0%

azetidine-2-carboxylic acid methyl ester hydrochloride (162698-26-2,51020-00-9) + benzenesulfonyl chloride (1939-99-7) → 1-Phenylmethanesulfonyl-azetidine-2-carboxylic acid methyl ester

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane;

upstream raw materials:

(2S)-Methyl-1-azetidine-2-carboxylic acid

methanol

Azetidine-2-carboxylic acid

Downstream raw materials:

azetidin-2-ylmethanol

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