4-BroMo-3,5-diMethylbenzyl alcohol

Base Information

• Chemical Name: 4-BroMo-3,5-diMethylbenzyl alcohol
• CAS No.: 27006-02-6
• Molecular Formula: C9H11BrO
• Molecular Weight: 215.09
• Hs Code.: 2906299090
• Mol file: 27006-02-6.mol

Synonyms:p-Brom-mesitylalkohol;4-bromo-3,5-dimethyl benzonitrile;4-Brom-11-oxy-1.3.5-trimethyl-benzol;4-bromo-3,5-dimethylbenzyl alcohol;4-Brom-3,5-dimethyl-benzonitril;4-Brom-3,5-dimethyl-benzylalkohol;

Chemical Property of 4-BroMo-3,5-diMethylbenzyl alcohol

Chemical Property:

• PSA: 20.23000
• LogP: 2.55820

Purity/Quality:

97% ^*data from raw suppliers

(4-Bromo-3,5-dimethylphenyl)methanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-BroMo-3,5-diMethylbenzyl alcohol

There total 8 articles about 4-BroMo-3,5-diMethylbenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(4-bromo-3,5-dimethylphenyl)methylene diacetate (74973-54-9) → (4-bromo-3,5-dimethylphenyl)methanol (27006-02-6)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; water; at 0 - 20 ℃; for 0.5h;

DOI:10.1016/j.bmcl.2013.09.035

Reference yield: 53.0%

2,4,6-trimethylphenyl bromide (576-83-0) → (4-bromo-3,5-dimethylphenyl)methanol (27006-02-6)

Guidance literature:

2,4,6-trimethylphenyl bromide; With chromium(VI) oxide; acetic anhydride; acetic acid;

With lithium aluminium tetrahydride;

DOI:10.1055/s-2006-944190

Reference yield: 10.0%

2,4,6-trimethylphenyl bromide (576-83-0) → (4-bromo-3,5-dimethylphenyl)methanol (27006-02-6) + 4-bromo-3,5-dimethylbenzaldehyde (400822-47-1)

Guidance literature:

With lead dioxide; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 40h;

DOI:10.1134/S1070428018030053

upstream raw materials:

4-bromo-3,5-dimethylbenzoic acid

2,4,6-trimethylphenyl bromide

(4-bromo-3,5-dimethylphenyl)methylene diacetate

2,5-dibromo-1,3-dimethylbenzene

Downstream raw materials:

2-bromo-5-(bromomethyl)-1,3-dimethylbenzene

4-(4-bromo-3,5-dimethylphenyl)butan-2-one