tert-Butyl 2-benzyl-2,7-diazaspiro[3.5]nonane-7-carboxylate

Base Information

• Chemical Name: tert-Butyl 2-benzyl-2,7-diazaspiro[3.5]nonane-7-carboxylate
• CAS No.: 1206969-92-7
• Molecular Formula: C19H28N2O2
• Molecular Weight: 316.444
• Hs Code.: 2933990090
• Mol file: 1206969-92-7.mol

Synonyms:tert-butyl 2-benzyl-2,7-diazaspiro[3.5]nonane-7-carboxylate;2-(Phenylmethyl)-2,7-diazaspiro[3.5]nonane-7-carboxylic acid tert-butyl ester

Chemical Property of tert-Butyl 2-benzyl-2,7-diazaspiro[3.5]nonane-7-carboxylate

Chemical Property:

• PSA: 32.78000
• Density: 1.12
• LogP: 3.39530

Purity/Quality:

97% ^*data from raw suppliers

7-CBZ-2,7-diaza-spiro[3.5]nonane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-Butyl 2-benzyl-2,7-diazaspiro[3.5]nonane-7-carboxylate

There total 2 articles about tert-Butyl 2-benzyl-2,7-diazaspiro[3.5]nonane-7-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,7-diaza-spiro[3.5]nonane-7-carboxylic acid tert-butyl ester (896464-16-7) + benzyl bromide (100-39-0) → C19H28N2O2 (1206969-92-7)

Guidance literature:

With potassium carbonate; In acetonitrile; at 20 ℃; for 2h;

Reference yield:

2,7-diaza-spiro[3.5]nonane-7-carboxylic acid tert-butyl ester (896464-16-7) + benzaldehyde (100-52-7) → C19H28N2O2 (1206969-92-7)

Guidance literature:

With sodium tris(acetoxy)borohydride;

DOI:10.1016/j.bmcl.2012.05.024

Reference yield: 63.5%

C19H28N2O2 (1206969-92-7) → C19H26N2O3

Guidance literature:

With ruthenium(IV) oxide; sodium periodate; In water; ethyl acetate; at 0 - 10 ℃; for 36h;

upstream raw materials:

2,7-diaza-spiro[3.5]nonane-7-carboxylic acid tert-butyl ester

benzaldehyde

benzyl bromide

Downstream raw materials:

C₁₄H₂₀N₂

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