3H-Indolium, 2-[2-[2-(diphenylphosphino)-3-[(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-ind ol-2-ylidene)ethylidene]-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-, iodide

Base Information

Chemical Name:3H-Indolium, 2-[2-[2-(diphenylphosphino)-3-[(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-ind ol-2-ylidene)ethylidene]-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-, iodide
CAS No.:144095-83-0
Molecular Formula:C46H50N2P.I
Molecular Weight:788.795
Hs Code.:

3H-Indolium, 2-[2-[2-(diphenylphosphino)-3-[(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-ind ol-2-ylidene)ethylidene]-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-, iodide

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Suppliers and Price of 3H-Indolium, 2-[2-[2-(diphenylphosphino)-3-[(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-ind ol-2-ylidene)ethylidene]-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-, iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3H-Indolium, 2-[2-[2-(diphenylphosphino)-3-[(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-ind ol-2-ylidene)ethylidene]-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-, iodide

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Technology Process of 3H-Indolium, 2-[2-[2-(diphenylphosphino)-3-[(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-ind ol-2-ylidene)ethylidene]-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-, iodide

There total 3 articles about 3H-Indolium, 2-[2-[2-(diphenylphosphino)-3-[(1-ethyl-1,3-dihydro-3,3-dimethyl-2H-ind ol-2-ylidene)ethylidene]-1-cyclohexen-1-yl]ethenyl]-1-ethyl-3,3-dimethyl-, iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 124591-86-2
2-<4'-chloro-7'-(1''-ethyl-3'',3''-dimethylindolin-2''ylidene)-3',5'-(propane-1''',3'''-diyl)-1',3',5'-heptatrien-1'-yl>-1-ethyl-3,3-dimethyl-3H-indolium iodide

: 829-85-6
diphenylphosphane

: 144095-83-0
2-<4'diphenylphosphino-7'-(1''-ethyl-3'',3''-dimethylindolin-2''-ylidene)-3',5'-(propane-1''',3'''-diyl)-1',3',5'-heptatrien-1'-yl>-1-ethyl-3,3-dimethylindolinium iodide

Guidance literature:: In N,N-dimethyl-formamide; at 100 ℃; for 2h;
DOI:10.1080/00397919208021656

Reference yield:

: 14134-81-7
1-ethyl-2,3,3-trimethylindolium iodide

: 144095-83-0
2-<4'diphenylphosphino-7'-(1''-ethyl-3'',3''-dimethylindolin-2''-ylidene)-3',5'-(propane-1''',3'''-diyl)-1',3',5'-heptatrien-1'-yl>-1-ethyl-3,3-dimethylindolinium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / AcONa / ethanol / 1 h / 80 °C

2: 68 percent / dimethylformamide / 2 h / 100 °C

With sodium acetate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1080/00397919208021656

Reference yield:

: 195382-10-6
N-<5-anilino-3-chloro-2,4-(propane-1',3'-diyl)-2,4-pentadien-1-ylidene>anilinium chloride

: 144095-83-0
2-<4'diphenylphosphino-7'-(1''-ethyl-3'',3''-dimethylindolin-2''-ylidene)-3',5'-(propane-1''',3'''-diyl)-1',3',5'-heptatrien-1'-yl>-1-ethyl-3,3-dimethylindolinium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / AcONa / ethanol / 1 h / 80 °C

2: 68 percent / dimethylformamide / 2 h / 100 °C

With sodium acetate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1080/00397919208021656