3H-Indolium, 1-ethyl-2,3,3-trimethyl-, iodide

Base Information

Chemical Name:3H-Indolium, 1-ethyl-2,3,3-trimethyl-, iodide
CAS No.:14134-81-7
Molecular Formula:C13H18N.I
Molecular Weight:315.197
Hs Code.:2933990090
DSSTox Substance ID:DTXSID90433924
ChEMBL ID:CHEMBL2393300
Mol file:14134-81-7.mol

Synonyms:14134-81-7;3H-Indolium, 1-ethyl-2,3,3-trimethyl-, iodide;1-Ethyl-2,3,3-trimethyl-3H-indol-1-ium iodide;1-Ethyl-2,3,3-trimethylindolenium Iodide;3H-Indolium, 1-ethyl-2,3,3-trimethyl-, iodide (1:1);1-ethyl-2,3,3-trimethylindol-1-ium;iodide;1-Ethyl-2,3,3-trimethyl-3H-indolium Iodide;42846-17-3;SCHEMBL2320529;YSZC1875;CHEMBL2393300;DTXSID90433924;MFCD00227166;AKOS024331518;AS-76501;CS-0153894;FT-0667999;D94515

Suppliers and Price of 3H-Indolium, 1-ethyl-2,3,3-trimethyl-, iodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
1-Ethyl-2,3,3-trimethylindolenium iodide
10mg
$ 403.00

TRC
1-Ethyl-2,3,3-trimethylindoleniumIodide
50mg
$ 200.00

Ambeed
1-Ethyl-2,3,3-trimethyl-3H-indol-1-iumiodide 97%
1g
$ 165.00

Ambeed
1-Ethyl-2,3,3-trimethyl-3H-indol-1-iumiodide 97%
5g
$ 563.00

Ambeed
1-Ethyl-2,3,3-trimethyl-3H-indol-1-iumiodide 97%
250mg
$ 65.00

aablocks
3H-Indolium,1-ethyl-2,3,3-trimethyl-,iodide(1:1) 97%
5g
$ 682.00

aablocks
3H-Indolium,1-ethyl-2,3,3-trimethyl-,iodide(1:1) 97%
250mg
$ 114.00

Total 9 raw suppliers

Chemical Property of 3H-Indolium, 1-ethyl-2,3,3-trimethyl-, iodide

Chemical Property:

Melting Point:165-166 °C
PSA：3.01000
LogP:0.06540
Storage Temp.:Refrigerator
Solubility.:Chloroform (Slightly), Methanol (Slightly)
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:315.04840
Heavy Atom Count:15
Complexity:262

Purity/Quality:

99%, ^*data from raw suppliers

1-Ethyl-2,3,3-trimethylindolenium iodide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC[N+]1=C(C(C2=CC=CC=C21)(C)C)C.[I-]
Uses Astrophloxine intermediate.

Technology Process of 3H-Indolium, 1-ethyl-2,3,3-trimethyl-, iodide

There total 9 articles about 3H-Indolium, 1-ethyl-2,3,3-trimethyl-, iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1640-39-7
2,3,3-trimethylindoleniune

: 75-03-6
ethyl iodide

: 14134-81-7
1-ethyl-2,3,3-trimethylindolium iodide

Guidance literature:: In neat (no solvent); at 120 - 140 ℃; for 0.333333h; Temperature; Microwave irradiation; Green chemistry;
DOI:10.1016/j.dyepig.2014.07.035

Reference yield:

: 73718-62-4
3,3-dimethyl-2-methylene-1-ethyl-2,3-dihydro-1H-indole

: 144-48-9
iodacetamide

: 122275-78-9
3,3-dimethyl-5'-oxo-1-ethyl-1,3-dihydrospiro<2H-indole-2,2'-pyrrolidine>

: 14134-81-7
1-ethyl-2,3,3-trimethylindolium iodide

Guidance literature:: In 1,4-dioxane; at 95 - 100 ℃; for 5.5h;
DOI:10.1007/BF00472617

Reference yield:

: 563-80-4
3-methyl-butan-2-one

: 14134-81-7
1-ethyl-2,3,3-trimethylindolium iodide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4 h / 70 - 80 °C

1.2: 4 h / 90 °C / oil bath

2.1: toluene / 7 h / Reflux; Inert atmosphere

In toluene; 1.1: Fischer Indole Synthesis / 1.2: Fischer Indole Synthesis;