DIPHENYL-4-D1

Base Information

Chemical Name:DIPHENYL-4-D1
CAS No.:4819-98-1
Molecular Formula:C6H5C6H4D
Molecular Weight:155.203
Hs Code.:
Mol file:4819-98-1.mol

Synonyms:4-deuterio-pyridine;biphenyl-4-d1;Nicotinsaeure-4-D;Niacin-d1;4-deuterio-nicotinic acid;4-deuterobiphenyl;Apelagrin-d1;Niacor-d1;Pelonin-d1;Wampocap-d1;4-Deuterio-pyridin;4-deuterio-biphenyl;Niaspan-d1;Akotin-d1;Nicotinic Acid-d1;4-Deuterio-nicotinsaeure;4d-pyridine;biphenyl-4-d;Nicacid-d1;

Suppliers and Price of DIPHENYL-4-D1

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
BIPHENYL-4-D1 95.00%
5MG
$ 497.27

Total 2 raw suppliers

Chemical Property of DIPHENYL-4-D1

Chemical Property:

PSA：0.00000
LogP:3.35360

Purity/Quality:

98% atom D ^*data from raw suppliers

BIPHENYL-4-D1 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of DIPHENYL-4-D1

There total 1 articles about DIPHENYL-4-D1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92-93-3
1-phenyl-4-nitrobenzene

: 17498-07-6
1-deuteriodiphenylmethanol

: 119-61-9
benzophenone

: 4819-98-1
[4-²H]biphenyl

Guidance literature:: With potassium phosphate; bis(acetylacetonato)palladium(II); dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine; In 1,4-dioxane; at 130 ℃; for 4h;
DOI:10.1021/acs.orglett.8b00430

Reference yield:

: potassium graphite

: UI(NCtBuMes)3(DME)

: 4819-98-1
[4-²H]biphenyl

: K2[(μ-η6,η6-biphenyl-4-d1)[U(NCtBuMes)3]2]

Guidance literature:: In 1,2-dimethoxyethane; (drybox, Schlenk, Ar) KC8 in DME was frozen, the thawing slurry was added dropwise to a frozen soln. of U-complex and biphenyl in DME, the mixt.was stirred at ca. 25°C for 25 min; filtered, the solvent was removed, extd. with pentane, filtered, evapd. to dryness, mixed with diethyl ether, stored for several days at -35°C, decanted, dried;
DOI:10.1021/ic202163m

Reference yield:

: potassium graphite

: UI(NCtBuMes)3(DME)

: 4819-98-1
[4-²H]biphenyl

: K[(μ-η6,η6-biphenyl-4-d1)[U(NCtBuMes)3]2]

Guidance literature:: In 1,2-dimethoxyethane; (drybox, Schlenk, Ar) KC8 in DME was frozen, the thawing slurry was added dropwise to a frozen soln. of U-complex and biphenyl-d10 in DME, the mixt. was stirred for 20 min; filtered, the solvent was removed, extd. with pentane, filtered, the solvent was removed, dissolved mixt. of pentane and diethyl ether, stored at -35°C for 3 d, crystals were dried under reduced pressure;
DOI:10.1021/ic202163m