2-Methylpropyl-d9-amine

Base Information

• Chemical Name: 2-Methylpropyl-d9-amine
• CAS No.: 1146967-64-7
• Molecular Formula: (CD3)2CDCD2NH2
• Molecular Weight: 82.0666
• Mol file: 1146967-64-7.mol

Synonyms:2-(methylpropyl-d9)-amine;

Chemical Property of 2-Methylpropyl-d9-amine

Chemical Property:

• PSA: 26.02000
• LogP: 1.30140
• Storage Temp.: Refrigerator
• Solubility.: Chloroform

Purity/Quality:

97% ^*data from raw suppliers

2-Methylpropyl-d9-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: Labelled 2-Methylpropylamine is used in the synthesis of arylsulfonamide inhibitors that act upon afflictions of osteoarthritis. In addition, it is used in the synthesis of novel reservatrol amide derivatives that act as anti-tumor agents. 2-METHYLPROPYL-D9-AMINE is used in the synthesis of arylsulfonamide inhibitors that act upon afflictions of osteoarthritis. In addition, it is used in the synthesis of novel reservatrol amide derivatives that act as anti-tumor agents.

Technology Process of 2-Methylpropyl-d9-amine

There total 1 articles about 2-Methylpropyl-d9-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(isobutyr-d7)-amide (1224439-42-2) → 2-methyl-1-propanamine-d9 (1146967-64-7)

Guidance literature:

With deutero lithium aluminiumhydride; In tetrahydrofuran; at 0 - 50 ℃; for 2h;

DOI:10.1016/j.ejmech.2013.02.001

Reference yield: 75.0%

2-methyl-1-propanamine-d9 (1146967-64-7) + (2R,3S)-3-[N-(tert-butyloxycarbonyl)amino]-1,2-epoxy-4-phenylbutane (98760-08-8) → tert-butyl (2S,3R)-3-hydroxy-4-((isobutyl-d9)-amino)-1-phenyIbutan-2-ylcarbamate (1146967-61-4)

Guidance literature:

In isopropyl alcohol; at 65 ℃; for 15h;

Reference yield:

2-methyl-1-propanamine-d9 (1146967-64-7) + tert-butyl ((S)-2-(4-(benzyloxy)phenyl)-1-((S)-oxiran-2-yl)ethyl)carbamate-d1 (1443118-23-7) → C26H28(2)H10N2O4

Guidance literature:

In tetrahydrofuran; at 50 ℃; for 48h; stereoselective reaction;

DOI:10.1016/j.ejmech.2013.02.001

upstream raw materials:

(isobutyr-d7)-amide

Downstream raw materials:

tert-butyl (2S,3R)-3-hydroxy-4-((isobutyl-d9)-amino)-1-phenyIbutan-2-ylcarbamate

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