2-Pyridinecarboxylicacid,5-methoxy-6-nitro-(9CI)

Base Information

• Chemical Name: 2-Pyridinecarboxylicacid,5-methoxy-6-nitro-(9CI)
• CAS No.: 324028-85-5
• Molecular Formula: C7H6N2O5
• Molecular Weight: 198.13
• Hs Code.: 2933399090
• Mol file: 324028-85-5.mol

Synonyms:2-Pyridinecarboxylicacid,5-methoxy-6-nitro-(9CI);5-Methoxy-6-nitropyridine-2-carboxylic acid;5-Methoxy-6-nitropicolinic acid;2-Pyridinecarboxylic acid, 5-Methoxy-6-nitro-

Chemical Property of 2-Pyridinecarboxylicacid,5-methoxy-6-nitro-(9CI)

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 433.234°C at 760 mmHg
• Flash Point: 215.812°C
• PSA: 105.24000
• Density: 1.512g/cm³
• LogP: 1.21980
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

5-methoxy-6-nitropicolinicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Pyridinecarboxylicacid,5-methoxy-6-nitro-(9CI)

There total 3 articles about 2-Pyridinecarboxylicacid,5-methoxy-6-nitro-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

5-methoxypyridine-2-carboxylic acid (29082-92-6) → 5-methoxy-6-nitropyridine-2-carboxylic acid (324028-85-5)

Guidance literature:

With Vilsmeier reagent; potassium nitrate; In neat (no solvent); at 100 ℃; under 1500.15 Torr; Reagent/catalyst; Temperature; Microwave irradiation;

DOI:10.1080/15533174.2012.752395

Reference yield: 12.3%

CH3 + 3-methoxy-6-methyl-2-nitro-pyridine (24015-98-3) → 5-methoxy-6-nitropyridine-2-carboxylic acid (324028-85-5)

Guidance literature:

With NO₂;

Reference yield:

3-methoxy-6-methyl-2-nitro-pyridine (24015-98-3) → 5-methoxy-6-nitropyridine-2-carboxylic acid (324028-85-5)

Guidance literature:

3-methoxy-6-methyl-2-nitro-pyridine; With potassium permanganate; water; at 75 ℃; for 18h;

With hydrogenchloride; water; at 0 ℃;

upstream raw materials:

3-methoxy-6-methyl-2-nitro-pyridine

5-methoxypyridine-2-carboxylic acid

Downstream raw materials:

5-methoxy-6-nitro-pyridine-2-carboxylic acid methyl ester

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