Methyl 5-Methoxy-6-nitropicolinate

Base Information

• Chemical Name: Methyl 5-Methoxy-6-nitropicolinate
• CAS No.: 390816-44-1
• Molecular Formula: C8H8N2O5
• Molecular Weight: 212.16000
• Hs Code.: 2933399090
• Mol file: 390816-44-1.mol

Synonyms:methyl 5-methoxy-6-nitropyridine-2-carboxylate;

Chemical Property of Methyl 5-Methoxy-6-nitropicolinate

Chemical Property:

• Boiling Point: 380.9±37.0 °C(Predicted)
• PKA: -3.24±0.10(Predicted)
• PSA: 94.24000
• Density: 1.356±0.06 g/cm3(Predicted)
• LogP: 1.30820
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

Methyl5-methoxy-6-nitropicolinate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 5-Methoxy-6-nitropicolinate

There total 4 articles about Methyl 5-Methoxy-6-nitropicolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-methoxy-6-nitropyridine-2-carboxylic acid (324028-85-5) + methyl iodide (74-88-4) → 5-methoxy-6-nitro-pyridine-2-carboxylic acid methyl ester (390816-44-1)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 48h;

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 3-methoxy-6-methyl-2-nitro-pyridine (24015-98-3) → 5-methoxy-6-nitro-pyridine-2-carboxylic acid methyl ester (390816-44-1)

Guidance literature:

With ammonia; In diethyl ether; water; magnesium sulfate;

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 5-methoxy-6-nitropyridine-2-carboxylic acid (324028-85-5) → 5-methoxy-6-nitro-pyridine-2-carboxylic acid methyl ester (390816-44-1)

Guidance literature:

In methanol; diethyl ether; dichloromethane; Heating / reflux;

upstream raw materials:

diazomethane

5-methoxy-6-nitropyridine-2-carboxylic acid

3-methoxy-6-methyl-2-nitro-pyridine

methyl iodide

Downstream raw materials:

5-cyclohexylamino-6-nitro-pyridine-2-carboxylic acid methyl ester

6-amino-5-methoxy-pyridine-2-carboxylic acid methyl ester

C₁₅H₁₅N₃O₅

C₁₆H₁₇N₃O₆

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