6H-Dibenz[c,e][1,2]oxaphosphorin, 6-hydroxy-, 6-oxide

Base Information

• Chemical Name: 6H-Dibenz[c,e][1,2]oxaphosphorin, 6-hydroxy-, 6-oxide
• CAS No.: 36240-31-0
• Molecular Formula: C12H9O3P
• Molecular Weight: 232.175
• DSSTox Substance ID: DTXSID50872794
• Nikkaji Number: J1.912.094E
• Wikidata: Q81978480
• Mol file: 36240-31-0.mol

Synonyms:DOPO-OH;6-hydroxy-6H-dibenzo [c,e][1,2]oxaphosphinine 6-oxide;dibenzo[c,e][1,2]oxaphosphinic acid;6-oxo-6H-6λ5-dibenzo[c,e][1,2]oxaphosphinin-6-ol;10-Oxo-10H-9-oxa-10λ5-phospha-phenanthren-10-ol;9,10-dihydro-10-hydroxy-9-oxa-10-phosphaphenanthrene-10-oxide;9,10-DIHYDRO-10-HYDROXY-9-OXA-10-PHOSPHA-PHENANTHRENE-10-ONE;

Chemical Property of 6H-Dibenz[c,e][1,2]oxaphosphorin, 6-hydroxy-, 6-oxide

Chemical Property:

• Melting Point: 203 °C (acetic acid)
• PSA: 56.34000
• LogP: 2.55670
• XLogP3: 2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 232.02893114
• Heavy Atom Count: 16
• Complexity: 317

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C3=CC=CC=C3P(=O)(O2)O

Technology Process of 6H-Dibenz[c,e][1,2]oxaphosphorin, 6-hydroxy-, 6-oxide

There total 1 articles about 6H-Dibenz[c,e][1,2]oxaphosphorin, 6-hydroxy-, 6-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

2-(Biphenyl-2-yloxy)-[1,3,2]dioxaphospholane (108881-14-7) → ethene (74-85-1) + 9,10-dihydro-10-hydroxy-9-oxa-10-phosphaphenanthrene-10-oxide (36240-31-0)

Guidance literature:

at 700 ℃; under 0.001 Torr;

DOI:10.1039/c39860001685

Reference yield: 94.0%

Diphenyliodonium triflate (66003-76-7) + 9,10-dihydro-10-hydroxy-9-oxa-10-phosphaphenanthrene-10-oxide (36240-31-0) → 6-phenoxy-6H-dibenzo[c,e][1,2]oxaphosphinine 6-oxide (55217-59-9)

Guidance literature:

With triethylamine; In toluene; at 110 ℃; for 3h; Inert atmosphere;

DOI:10.1021/cs501523g

upstream raw materials:

2-(Biphenyl-2-yloxy)-[1,3,2]dioxaphospholane

Downstream raw materials:

6-phenoxy-6H-dibenzo[c,e][1,2]oxaphosphinine 6-oxide

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