Ethyl 2-(5-bromobenzo[b]thiophen-3-yl)acetate

Base Information

Chemical Name:Ethyl 2-(5-bromobenzo[b]thiophen-3-yl)acetate
CAS No.:17266-44-3
Molecular Formula:C₁₂H₁₁BrO₂S
Molecular Weight:299.188
Hs Code.:2934999090
Mol file:17266-44-3.mol

Synonyms:ethyl 2-(5-broMobenzo[b]thiophen-3-yl)acetate;Ethyl (5-bromobenzothiophen-3-yl)acetate

Suppliers and Price of Ethyl 2-(5-bromobenzo[b]thiophen-3-yl)acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Ethyl2-(5-bromobenzo[b]thiophen-3-yl)acetate 95+%
1g
$ 650.00

Chemenu
ethyl2-(5-bromobenzo[b]thiophen-3-yl)acetate 95%
5g
$ 1059.00

Chemenu
ethyl2-(5-bromobenzo[b]thiophen-3-yl)acetate 95%
1g
$ 354.00

Alichem
Ethyl2-(5-bromobenzo[b]thiophen-3-yl)acetate
1g
$ 400.00

Total 9 raw suppliers

Chemical Property of Ethyl 2-(5-bromobenzo[b]thiophen-3-yl)acetate

Chemical Property:

PSA：54.54000
Density:1.507
LogP:3.76940
Storage Temp.:2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

Ethyl2-(5-bromobenzo[b]thiophen-3-yl)acetate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethyl 2-(5-bromobenzo[b]thiophen-3-yl)acetate

There total 5 articles about Ethyl 2-(5-bromobenzo[b]thiophen-3-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.8%

: 130106-00-2
4-((4-bromophenyl)thio)-3-oxobutanoic acid ethyl ester

: 17266-44-3
ethyl 2-(5-bromobenzo[b]thiophen-3-yl)acetate

Guidance literature:: With polyphosphoric acid; In toluene; at 100 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.ejmech.2017.03.037

Reference yield: 61.8%

: 17266-44-3
ethyl 2-(5-bromobenzo[b]thiophen-3-yl)acetate

Guidance literature:: With polyphosphoric acid; In toluene; at 100 ℃; Inert atmosphere;

Reference yield:

: 638-07-3
ethyl (2-chloroaceto)acetate

: 106-53-6
para-bromobenzenethiol

: 17266-44-3
ethyl 2-(5-bromobenzo[b]thiophen-3-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 0 °C

2: polyphosphoric acid / toluene / 16 h / 100 °C / Inert atmosphere

With triethylamine; In dichloromethane; toluene;
DOI:10.1016/j.ejmech.2017.03.037