cis-2-(2-Buten-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:cis-2-(2-Buten-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:167773-12-8
Molecular Formula:C10H19BO2
Molecular Weight:182.071
Hs Code.:
Mol file:167773-12-8.mol

Synonyms:CIS-2-(2-BUTEN-1-YL)-4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLANE;E-Crotylboronic acidpinacol ester;2--4,4,5,5-tetraMethyl-1,3,2-dioxaborolane

Suppliers and Price of cis-2-(2-Buten-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
2-(But-2-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
5g
$ 2363.76

Alichem
2-(But-2-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
1g
$ 884.40

Total 5 raw suppliers

Chemical Property of cis-2-(2-Buten-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Chemical Property:

Boiling Point:195.5±19.0 °C(Predicted)
PSA：18.46000
Density:0.89±0.1 g/cm3(Predicted)
LogP:2.65470

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-(But-2-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of cis-2-(2-Buten-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 2 articles about cis-2-(2-Buten-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6117-91-5,542-72-3
(E/Z)-2-buten-1-ol

: 73183-34-3
bis(pinacol)diborane

: 167773-12-8
2-<(2E/Z)-2-butenyl>-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With bis[(benzyldimethylamino)chloropalladium(II)]; toluene-4-sulfonic acid; In methanol; dimethyl sulfoxide; at 50 ℃; for 12h;
DOI:10.1002/chem.201704760

Reference yield:

: 624-64-6
trans-2-Butene

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 167773-12-8
2-<(2E/Z)-2-butenyl>-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: trans-2-Butene; With n-butyllithium; potassium tert-butylate; In tetrahydrofuran; hexane; at -78 - -45 ℃; Inert atmosphere;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; hexane; dichloromethane; water; for 0.5h; Saturated solution;
DOI:10.1021/jo802215v