4-Bromo-2-iodo-1-(trifluoromethyl)benzene

Base Information

• Chemical Name: 4-Bromo-2-iodo-1-(trifluoromethyl)benzene
• CAS No.: 1256945-00-2
• Molecular Formula: C7H3BrF3I
• Molecular Weight: 350.905
• Hs Code.: 2903999090
• Mol file: 1256945-00-2.mol

Synonyms:4-BroMo-2-iodo-1-(trifluoroMethyl)benzene;4-BroMo-2-iodobenzotrifluoride

Chemical Property of 4-Bromo-2-iodo-1-(trifluoromethyl)benzene

Chemical Property:

• Boiling Point: 264.1±40.0 °C(Predicted)
• PSA: 0.00000
• Density: 2.176±0.06 g/cm3(Predicted)
• LogP: 4.07250
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

99%, ^*data from raw suppliers

4-Bromo-2-iodo-1-(trifluoromethyl)benzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Bromo-2-iodo-1-(trifluoromethyl)benzene

There total 2 articles about 4-Bromo-2-iodo-1-(trifluoromethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

5-bromo-2-trifluoromethylphenylamine (703-91-3) → 4-bromo-2-iodo-1-(trifluoromethyl)benzene (1256945-00-2)

Guidance literature:

5-bromo-2-trifluoromethylphenylamine; With tert.-butylnitrite; boron trifluoride diethyl etherate; In tetrahydrofuran; at -78 - 20 ℃; for 0.666667h;

With iodine; potassium iodide; In acetone; at 0 - 20 ℃; for 1h;

Reference yield:

→ 4-bromo-2-iodo-1-(trifluoromethyl)benzene (1256945-00-2)

Guidance literature:

Reference yield: 76.0%

4-bromo-2-iodo-1-(trifluoromethyl)benzene (1256945-00-2) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → 3-(5-bromo-2-(trifluoromethyl)phenyl)acrylic acid methyl ester

Guidance literature:

With potassium carbonate; triethylamine; palladium diacetate; triphenylphosphine; In tetrahydrofuran; at 80 ℃; for 16h; Sealed tube;

upstream raw materials:

5-bromo-2-trifluoromethylphenylamine

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