Technology Process of D-102 Dye
There total 7 articles about D-102 Dye which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium tetrahydroborate; acetic acid / 20 °C
2.1: tri-tert-butyl phosphine; potassium tert-butylate; palladium diacetate / 5,5-dimethyl-1,3-cyclohexadiene / 120 °C
3.1: trichlorophosphate / 10 °C
3.2: 20 °C
4.1: ammonium acetate; acetic acid / 120 °C
With
sodium tetrahydroborate; tri-tert-butyl phosphine; potassium tert-butylate; ammonium acetate; palladium diacetate; acetic acid; trichlorophosphate;
In
5,5-dimethyl-1,3-cyclohexadiene;
DOI:10.1016/j.dyepig.2011.02.009
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tri-tert-butyl phosphine; potassium tert-butylate; palladium diacetate / 5,5-dimethyl-1,3-cyclohexadiene / 120 °C
2.1: trichlorophosphate / 10 °C
2.2: 20 °C
3.1: ammonium acetate; acetic acid / 120 °C
With
tri-tert-butyl phosphine; potassium tert-butylate; ammonium acetate; palladium diacetate; acetic acid; trichlorophosphate;
In
5,5-dimethyl-1,3-cyclohexadiene;
DOI:10.1016/j.dyepig.2011.02.009
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium acetate; acetic acid / dichloromethane; water / 2 h / Reflux
2.1: sodium tetrahydroborate; acetic acid / 20 °C
3.1: tri-tert-butyl phosphine; potassium tert-butylate; palladium diacetate / 5,5-dimethyl-1,3-cyclohexadiene / 120 °C
4.1: trichlorophosphate / 10 °C
4.2: 20 °C
5.1: ammonium acetate; acetic acid / 120 °C
With
sodium tetrahydroborate; tri-tert-butyl phosphine; potassium tert-butylate; ammonium acetate; sodium acetate; palladium diacetate; acetic acid; trichlorophosphate;
In
5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; water;
DOI:10.1016/j.dyepig.2011.02.009
