Acetic acid, chloro[(3-cyanophenyl)hydrazono]-, ethyl ester

Base Information

Chemical Name:Acetic acid, chloro[(3-cyanophenyl)hydrazono]-, ethyl ester
CAS No.:1217070-70-6
Molecular Formula:C11H10ClN3O2
Molecular Weight:251.672
Hs Code.:

Synonyms:Acetic acid,chloro[(3-cyanophenyl)hydrazono]-,ethyl ester;Acetic acid, 2-chloro-2-[2-(3-cyanophenyl)hydrazinylidene]-, ethyl ester

Suppliers and Price of Acetic acid, chloro[(3-cyanophenyl)hydrazono]-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of Acetic acid, chloro[(3-cyanophenyl)hydrazono]-, ethyl ester

Chemical Property:

PSA：74.48000
LogP:2.15858

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

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Technology Process of Acetic acid, chloro[(3-cyanophenyl)hydrazono]-, ethyl ester

There total 1 articles about Acetic acid, chloro[(3-cyanophenyl)hydrazono]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2237-30-1
m-cyanoaniline

: 609-15-4
ethyl 2-chloro-3-oxo-butyrate

: 1217070-70-6
ethyl 2-chloro-2-(2-(3-cyanophenyl)hydrazono)acetate

Guidance literature:: m-cyanoaniline; With sodium nitrite; In water; at -5 - 0 ℃; for 0.5h;

ethyl 2-chloro-3-oxo-butyrate; With sodium acetate; acetic acid; In water; at 0 ℃; for 1h;

Reference yield: 96.0%

: 473927-69-4
1-(4-iodo-phenyl)-3-morpholin-4-yl-5,6-dihydro-1H-pyridin-2-one

: 1217070-70-6
ethyl 2-chloro-2-(2-(3-cyanophenyl)hydrazono)acetate

: 1217070-71-7
C₂₂H₁₇IN₄O₃

Guidance literature:: With triethylamine; In toluene; Reflux;
DOI:10.1016/j.bmcl.2010.01.011

Reference yield: 44.0%

: 1217070-70-6
ethyl 2-chloro-2-(2-(3-cyanophenyl)hydrazono)acetate

: 5-(4-iodophenyl)-7-morpholino-5-azaspiro[2.5]oct-7-en-6-one

: ethyl 6-[4-iodophenyl]-1-(3-cyanophenyl)-7-oxospiro[5H-pyrazolo[3,4-c]pyridine-4,1'-cyclopropane]-3-carboxylate

Guidance literature:: ethyl 2-chloro-2-(2-(3-cyanophenyl)hydrazono)acetate; 5-(4-iodophenyl)-7-morpholino-5-azaspiro[2.5]oct-7-en-6-one; With triethylamine; potassium iodide; In ethyl acetate; at 75 ℃;

With hydrogenchloride; In water; ethyl acetate; at 65 ℃; for 7h;