4-Hydroxymethyl-1-methyl-2-piperidone

Base Information

• Chemical Name: 4-Hydroxymethyl-1-methyl-2-piperidone
• CAS No.: 20845-32-3
• Molecular Formula: C7H13NO2
• Molecular Weight: 143.186
• Hs Code.: 2933790090
• Mol file: 20845-32-3.mol

Synonyms:4-(hydroxymethyl)-1-methylpiperidin-2-one;

Chemical Property of 4-Hydroxymethyl-1-methyl-2-piperidone

Chemical Property:

• PSA: 40.54000
• LogP: -0.21500
• Storage Temp.: 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

4-(Hydroxymethyl)-1-methylpiperidin-2-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Hydroxymethyl-1-methyl-2-piperidone

There total 2 articles about 4-Hydroxymethyl-1-methyl-2-piperidone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1-methyl-4-piperidinemethanol (20691-89-8) → 1-methylpiperidine-4-carboxylic acid (68947-43-3) + 4-(hydroxymethyl)-1-methyl-2-piperidinone (20845-32-3)

Guidance literature:

With water; oxygen; at 60 ℃; for 24h; under 760.051 Torr; regioselective reaction; Green chemistry;

DOI:10.1002/anie.201602695

Reference yield:

→ 4-(hydroxymethyl)-1-methyl-2-piperidinone (20845-32-3)

Guidance literature:

/BRN= 473824/, LiAlH4, Ae.;

upstream raw materials:

1-methyl-4-piperidinemethanol

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