1-(2-methoxy-4-nitrophenyl)-4-methyl-1H-imidazole

Base Information

• Chemical Name: 1-(2-methoxy-4-nitrophenyl)-4-methyl-1H-imidazole
• CAS No.: 958245-17-5
• Molecular Formula: C11H11N3O3
• Molecular Weight: 233.227
• Hs Code.: 2933290090
• Mol file: 958245-17-5.mol

Synonyms:1-(2-Methoxy-4-nitrophenyl)-4-methyl-1H-imidazol; 1-(2-methoxy-4-nitrophenyl)-4-methyl-1H-imidazole; 1H-imidazole, 1-(2-methoxy-4-nitrophenyl)-4-methyl-

Chemical Property of 1-(2-methoxy-4-nitrophenyl)-4-methyl-1H-imidazole

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 439.602°C at 760 mmHg
• PKA: 5.10±0.61(Predicted)
• Flash Point: 219.663°C
• PSA: 72.87000
• Density: 1.308g/cm³
• LogP: 2.62070
• Storage Temp.: 2-8°C

Purity/Quality:

NLT 98% ^*data from raw suppliers

1-(2-Methoxy-4-nitrophenyl)-4-methyl-1H-imidazole 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(2-methoxy-4-nitrophenyl)-4-methyl-1H-imidazole

There total 4 articles about 1-(2-methoxy-4-nitrophenyl)-4-methyl-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

4-methyl-1H-imidazole (822-36-6) + 2-chloro-5-nitroanisole (1009-36-5) → 1-(2-methoxy-4-nitrophenyl)-4-methyl-1H-imidazole (958245-17-5)

Guidance literature:

With potassium hydroxide; In dimethyl sulfoxide; at 80 ℃; for 8h; Inert atmosphere;

Reference yield: 79.0%

4-methyl-1H-imidazole (822-36-6) + 1-fluoro-2-methoxy-4-nitrobenzene (454-16-0) → 1-(2-methoxy-4-nitrophenyl)-4-methyl-1H-imidazole (958245-17-5)

Guidance literature:

With potassium carbonate; In dimethyl sulfoxide; at 125 ℃; for 16h; Autoclave; Inert atmosphere;

Reference yield:

4-methyl-1H-imidazole (822-36-6) + 1-bromo-2-methoxy-4-nitrobenzene (77337-82-7) → 1-(2-methoxy-4-nitrophenyl)-4-methyl-1H-imidazole (958245-17-5)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 - 70 ℃; for 3h;

upstream raw materials:

4-methyl-1H-imidazole

2-chloro-5-nitroanisole

1-bromo-2-methoxy-4-nitrobenzene

1-fluoro-2-methoxy-4-nitrobenzene

Downstream raw materials:

3-methoxy-4-(5-methyl-1H-imidazol-1-yl)aniline

3-methoxy-4-(4-methyl-1H-imidazol-1-yl)benzoic acid

[8-(4-fluoro-phenyl)-5,6,7,8-tetrahydro-[1,2,4]-triazolo[1,5-a]pyridin-2-yl]-[3-methoxy-4-(4-methyl-imidazol-1-yl)-phenyl]-amine

8-[4-fluoro-2-(trifluoromethyl)phenyl]-N-[3-methoxy-4-(4-methyl-1H-imidazol-1-yl)phenyl]-[1,2,4]triazolo[1,5-a]pyridin-2-amine

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