Diethyl 2-(3,5-diiodo-4-(4-Methoxyphenoxy)benzyl)Malonate

Base Information

Chemical Name:Diethyl 2-(3,5-diiodo-4-(4-Methoxyphenoxy)benzyl)Malonate
CAS No.:94861-76-4
Molecular Formula:C₂₁H₂₂I₂O₆
Molecular Weight:624.211
Hs Code.:2918990090
Mol file:94861-76-4.mol

Synonyms:[3,5-diiodo-4-(4-methoxy-phenoxy)-benzyl]-malonic acid diethyl ester;S06-0018;diethyl 2-(3,5-diiodo-4-(4-methoxyphenoxy)benzyl)malonate;[3,5-Dijod-4-(4-methoxy-phenoxy)-benzyl]-malonsaeure-diaethylester;

Suppliers and Price of Diethyl 2-(3,5-diiodo-4-(4-Methoxyphenoxy)benzyl)Malonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Diethyl2-(3,5-diiodo-4-(4-methoxyphenoxy)benzyl)malonate 95+%
1g
$ 561.00

American Custom Chemicals Corporation
DIETHYL 2-(3,5-DIIODO-4-(4-METHOXYPHENOXY)BENZYL)MALONATE 95.00%
10G
$ 1334.03

American Custom Chemicals Corporation
DIETHYL 2-(3,5-DIIODO-4-(4-METHOXYPHENOXY)BENZYL)MALONATE 95.00%
5G
$ 909.56

Total 14 raw suppliers

Chemical Property of Diethyl 2-(3,5-diiodo-4-(4-Methoxyphenoxy)benzyl)Malonate

Chemical Property:

PSA：71.06000
LogP:4.98160
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Diethyl2-(3,5-diiodo-4-(4-methoxyphenoxy)benzyl)malonate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Diethyl 2-(3,5-diiodo-4-(4-Methoxyphenoxy)benzyl)Malonate

There total 6 articles about Diethyl 2-(3,5-diiodo-4-(4-Methoxyphenoxy)benzyl)Malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95281-79-1
[3,5-diamino-4-(4-methoxy-phenoxy)-benzyl]-malonic acid diethyl ester

: 94861-76-4
[3,5-diiodo-4-(4-methoxy-phenoxy)-benzyl]-malonic acid diethyl ester

Guidance literature:: With sulfuric acid; acetic acid; sodium nitrite; Behandeln der Bis-diazoniumsalz-Loesung mit NaI, Jod und Harnstoff in H₂O und CHCl₃;
DOI:10.1021/jo01363a010

Reference yield:

: 17315-86-5
2-(4-hydroxybenzylidene)malonic acid diethyl ester

: 94861-76-4
[3,5-diiodo-4-(4-methoxy-phenoxy)-benzyl]-malonic acid diethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: H₂SO₄ / -5 °C / anschliessend mit konz. wss. HNO₃ bei -15grad behandeln

2: methanesulfonyl chloride; pyridine / Reaktion ueber 2 Stufen

3: palladium/charcoal; acetic acid / Hydrogenation

4: NaNO₂; H₂SO₄; acetic acid / Behandeln der Bis-diazoniumsalz-Loesung mit NaI, Jod und Harnstoff in H₂O und CHCl₃

With pyridine; palladium on activated charcoal; sulfuric acid; acetic acid; methanesulfonyl chloride; sodium nitrite;
DOI:10.1021/jo01363a010

Reference yield:

: 100871-24-7
(4-hydroxy-3,5-dinitro-benzylidene)-malonic acid diethyl ester

: 94861-76-4
[3,5-diiodo-4-(4-methoxy-phenoxy)-benzyl]-malonic acid diethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: methanesulfonyl chloride; pyridine / Reaktion ueber 2 Stufen

2: palladium/charcoal; acetic acid / Hydrogenation

3: NaNO₂; H₂SO₄; acetic acid / Behandeln der Bis-diazoniumsalz-Loesung mit NaI, Jod und Harnstoff in H₂O und CHCl₃

With pyridine; palladium on activated charcoal; sulfuric acid; acetic acid; methanesulfonyl chloride; sodium nitrite;
DOI:10.1021/jo01363a010