Technology Process of cis-3-Hydroxy-3-MethylcyclobutylaMine
There total 5 articles about cis-3-Hydroxy-3-MethylcyclobutylaMine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
methanol;
for 16h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: water; potassium hydroxide / ethanol / 16 h / 80 °C
2.1: triethylamine; diphenyl phosphoryl azide / acetonitrile; 1,4-dioxane / 1 h / 75 °C
2.2: 16 h / 100 °C
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 27 °C
4.1: lithium triethylborohydride / tetrahydrofuran / 1 h / 0 - 27 °C
5.1: hydrogen; palladium 10% on activated carbon / ethanol / 5 h / 20 °C
With
diphenyl phosphoryl azide; palladium 10% on activated carbon; water; hydrogen; lithium triethylborohydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 27 °C
2: lithium triethylborohydride / tetrahydrofuran / 1 h / 0 - 27 °C
3: hydrogen; palladium 10% on activated carbon / ethanol / 5 h / 20 °C
With
palladium 10% on activated carbon; hydrogen; lithium triethylborohydride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; ethanol; dichloromethane;
