2-Chloro-5-methylbenzaldehyde

Base Information

• Chemical Name: 2-Chloro-5-methylbenzaldehyde
• CAS No.: 14966-09-7
• Molecular Formula: C8H7ClO
• Molecular Weight: 154.59358
• Hs Code.: 2913000090
• European Community (EC) Number: 690-762-6
• Mol file: 14966-09-7.mol

Synonyms:2-chloro-5-methylbenzaldehyde;14966-09-7;Benzaldehyde, 2-chloro-5-methyl-;SCHEMBL7689361;IMJCLRALWLMDCZ-UHFFFAOYSA-N;MFCD12025212;AKOS023428158;s10830;AS-19837;CS-0194931;EN300-57015;Z871801784

Chemical Property of 2-Chloro-5-methylbenzaldehyde

Chemical Property:

• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C
• XLogP3: 2.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 154.0185425
• Heavy Atom Count: 10
• Complexity: 124

Purity/Quality:

99% ^*data from raw suppliers

2-Chloro-5-methylbenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=C(C=C1)Cl)C=O

Technology Process of 2-Chloro-5-methylbenzaldehyde

There total 2 articles about 2-Chloro-5-methylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dichloromethyl methyl ether (4885-02-3) + para-chlorotoluene (106-43-4) → 5-chloro-2-methylbenzaldehyde (58966-34-0) + 2-chloro-5-methylbenzaldehyde (14966-09-7)

Guidance literature:

With titanium tetrachloride; In dichloromethane; at 20 ℃; for 15h;

Reference yield:

→ 2-chloro-5-methylbenzaldehyde (14966-09-7)

Guidance literature:

RNH2, HNO2, HC...?;

Reference yield: 91.0%

9H-fluorene (86-73-7) + 2-chloro-5-methylbenzaldehyde (14966-09-7) → 9-(2-chloro-5-methylbenzylidene)fluorene

Guidance literature:

With potassium tert-butylate; In tert-butyl alcohol; at 50 ℃; for 3h;

DOI:10.1021/jo00067a070

upstream raw materials:

Dichloromethyl methyl ether

para-chlorotoluene

Downstream raw materials:

4-(2-chloro-5-methylphenyl)-3-buten-2-one

4-chloro-3-(trichlorovinyl)toluene

C₃₅H₃₆N₂O₇

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