2-(((benzyloxy)carbonyl)amino)pyrimidine-4-carboxylic acid

Base Information

Chemical Name:2-(((benzyloxy)carbonyl)amino)pyrimidine-4-carboxylic acid
CAS No.:1443227-29-9
Molecular Formula:C₁₃H₁₁N₃O₄
Molecular Weight:273.248
Hs Code.:
Mol file:1443227-29-9.mol

Synonyms:2-(((benzyloxy)carbonyl)amino)pyrimidine-4-carboxylic acid

Suppliers and Price of 2-(((benzyloxy)carbonyl)amino)pyrimidine-4-carboxylic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 2-(((benzyloxy)carbonyl)amino)pyrimidine-4-carboxylic acid

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

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Technology Process of 2-(((benzyloxy)carbonyl)amino)pyrimidine-4-carboxylic acid

There total 3 articles about 2-(((benzyloxy)carbonyl)amino)pyrimidine-4-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1312764-26-3
benzyl (4-formylpyrimidin-2-yl)carbamate

: 1443227-29-9
2-(((benzyloxy)carbonyl)amino)pyrimidine-4-carboxylic acid

Guidance literature:: With potassium permanganate; In water; dimethyl sulfoxide; at 20 ℃; for 24h;
DOI:10.1016/j.tetlet.2013.05.026

Reference yield:

: 165807-05-6
4-(dimethoxymethyl)pyrimidin-2-amine

: 1443227-29-9
2-(((benzyloxy)carbonyl)amino)pyrimidine-4-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate / water; ethanol / 0.25 h

1.2: 12 h / 5 - 10 °C

2.1: hydrogenchloride / water / 5 h / 20 °C

3.1: potassium permanganate / water; dimethyl sulfoxide / 24 h / 20 °C

With hydrogenchloride; potassium permanganate; sodium hydrogencarbonate; In ethanol; water; dimethyl sulfoxide;
DOI:10.1016/j.tetlet.2013.05.026

Reference yield:

: 1312764-25-2
benzyl (4-(dimethoxymethyl)pyrimidin-2-yl)carbamate

: 1443227-29-9
2-(((benzyloxy)carbonyl)amino)pyrimidine-4-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water / 5 h / 20 °C

2: potassium permanganate / water; dimethyl sulfoxide / 24 h / 20 °C

With hydrogenchloride; potassium permanganate; In water; dimethyl sulfoxide;
DOI:10.1016/j.tetlet.2013.05.026