1-(8-Azidonaphthalen-1-yl)-1H-1,2,3-triazole-4-carboxylic acid ethyl ester

Base Information

• Chemical Name: 1-(8-Azidonaphthalen-1-yl)-1H-1,2,3-triazole-4-carboxylic acid ethyl ester
• CAS No.: 91165-56-9
• Molecular Formula: C₁₅H₁₂N₆O₂
• Molecular Weight: 308.299
• Mol file: 91165-56-9.mol

Synonyms:1-(8-Azidonaphthalen-1-yl)-1H-1,2,3-triazole-4-carboxylic acid ethyl ester

Chemical Property of 1-(8-Azidonaphthalen-1-yl)-1H-1,2,3-triazole-4-carboxylic acid ethyl ester

Chemical Property:

• PSA: 106.76000
• LogP: 2.99176

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

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Technology Process of 1-(8-Azidonaphthalen-1-yl)-1H-1,2,3-triazole-4-carboxylic acid ethyl ester

There total 3 articles about 1-(8-Azidonaphthalen-1-yl)-1H-1,2,3-triazole-4-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

1,8-diazidonaphthalene (22187-34-4) + propynoic acid ethyl ester (623-47-2) → ethyl-1-(8-azido-1-naphthyl)-1H-1,2,3-triazole-5-carboxylate (91165-58-1) + ethyl 1-(8-azido-1-naphthyl)-1H-1,2,3-triazole-4-carboxylate (91165-56-9)

Guidance literature:

In diethyl ether; for 24h; Ambient temperature; dark;

DOI:10.1246/bcsj.60.2931

Reference yield:

1,8-diazidonaphthalene (22187-34-4) + propynoic acid ethyl ester (623-47-2) → ethyl-1-(8-azido-1-naphthyl)-1H-1,2,3-triazole-5-carboxylate (91165-58-1) + ethyl 1-(8-azido-1-naphthyl)-1H-1,2,3-triazole-4-carboxylate (91165-56-9) + ethyl 1-<8-(5-ethoxycarbonyl-1H-1,2,3-triazol-1-yl)-1-naphthyl>-1H-1,2,3-triazole-4-carboxylate (91165-68-3) + diethyl 1,1'-(1,8-naphthylene)di-1H-1,2,3-triazole-4-carboxylate (91165-66-1)

Guidance literature:

for 336h; Further byproducts given; Ambient temperature;

DOI:10.1039/c39840000450

Reference yield:

1,8-diazidonaphthalene (22187-34-4) + propynoic acid ethyl ester (623-47-2) → ethyl 1-(8-azido-1-naphthyl)-1H-1,2,3-triazole-4-carboxylate (91165-56-9) + ethyl 1-<8-(5-ethoxycarbonyl-1H-1,2,3-triazol-1-yl)-1-naphthyl>-1H-1,2,3-triazole-4-carboxylate (91165-68-3) + diethyl 1,1'-(1,8-naphthylene)di-1H-1,2,3-triazole-5-carboxylate (91165-70-7) + diethyl 1,1'-(1,8-naphthylene)di-1H-1,2,3-triazole-4-carboxylate (91165-66-1)

Guidance literature:

for 336h; Further byproducts given; Ambient temperature;

DOI:10.1039/c39840000450

upstream raw materials:

1,8-diazidonaphthalene

propynoic acid ethyl ester

Downstream raw materials:

diethyl 1-<8-(4-ethoxycarbonyl-1H-1,2,3-triazole-1-yl)-1-naphthyl>-1H-1,2,3-triazole-4,5-dicarboxylate

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