3-BroMo-8-Methoxyquinoline

Base Information

• Chemical Name: 3-BroMo-8-Methoxyquinoline
• CAS No.: 103030-27-9
• Molecular Formula: C10H8BrNO
• Molecular Weight: 238.084
• Mol file: 103030-27-9.mol

Synonyms:3-BroMo-8-Methoxyquinoline

Chemical Property of 3-BroMo-8-Methoxyquinoline

Chemical Property:

• PSA: 22.12000
• LogP: 3.00590

Purity/Quality:

97% ^*data from raw suppliers

3-Bromo-8-methoxyquinoline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-BroMo-8-Methoxyquinoline

There total 3 articles about 3-BroMo-8-Methoxyquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.8%

8-hydroxy-3-bromoquinoline (139399-62-5) + methyl iodide (74-88-4) → 3-bromo-8-methoxyquinoline (103030-27-9)

Guidance literature:

8-hydroxy-3-bromoquinoline; With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 0.25h;

methyl iodide; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 15h;

Reference yield:

3-bromo-8-aminoquinoline (139399-67-0) → 3-bromo-8-methoxyquinoline (103030-27-9)

Guidance literature:

Multi-step reaction with 2 steps

1: water; sulfuric acid / 220 °C

2: water; NaOH-solution

With sodium hydroxide; sulfuric acid; water;

DOI:10.1039/jr9570000290

Reference yield:

8-hydroxy-3-bromoquinoline (139399-62-5) + dimethyl sulfate (77-78-1) → 3-bromo-8-methoxyquinoline (103030-27-9)

Guidance literature:

With sodium hydroxide; water;

DOI:10.1039/jr9570000290

upstream raw materials:

8-hydroxy-3-bromoquinoline

dimethyl sulfate

3-bromo-8-aminoquinoline

methyl iodide

Downstream raw materials:

C₁₇H₁₄FNO

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